2-溴-1,2-双-(4-甲氧基苯基)-乙酮合成路线 （共 13 条）
反应条件
pyridinium tribromide in dichloromethane T=20°C; 1 h;
参考文献
TORAY INDUSTRIES, INC.
Patent: EP2009006 A1, 2008 ;
Location in patent: Page/Page column 42-43 ;
反应条件
phosphorus tribromide in tetrachloromethane Heating;
参考文献
Seko; Yoshino; Yokota; Tsukamoto
Chemical and Pharmaceutical Bulletin, 1991 , vol. 39, # 3 p. 651 - 657
反应条件
triethylamine; dibromotriphenyl-phosphorane in dichloromethane T=20°C; Bromination; 24 h;
参考文献
Furukawa, Isao; Sasaki, Mitsuhiro; Inoue, Takeshi; Ohta, Tetsuo
Phosphorus, Sulfur and Silicon and Related Elements, 1998 , vol. 143, p. 85 - 99
反应条件
1: phosphoric acid; trifluoroacetic anhydride / 0.02 h / 25 °C 2: bromine / chloroform / 0.5 h / 50 °C View Scheme
参考文献
Palkar, Mahesh B.; Noolvi, Malleshappa N.; Maddi, Veeresh S.; Ghatole, Mangala; Nargund, Laxmivenkat G.
Medicinal Chemistry Research, 2012 , vol. 21, # 7 p. 1313 - 1321
反应条件
1: phosphoric acid; trifluoroacetic anhydride / 0.02 h / 25 °C 2: bromine / chloroform / 0.5 h / 50 °C View Scheme
参考文献
Palkar, Mahesh B.; Noolvi, Malleshappa N.; Maddi, Veeresh S.; Ghatole, Mangala; Nargund, Laxmivenkat G.
Medicinal Chemistry Research, 2012 , vol. 21, # 7 p. 1313 - 1321
参考文献
Henne; Bruylants
Bulletin des Societes Chimiques Belges, 1948 , vol. 57, p. 320,328
反应条件
in acetonitrile T=60°C;
参考文献
Seko; Yoshino; Yokota; Tsukamoto
Chemical and Pharmaceutical Bulletin, 1991 , vol. 39, # 3 p. 651 - 657
反应条件
4-methoxy pyridine; Ru(bpy)3Cl2; lithium carbonate in N,N-dimethyl acetamide T=25°C; 24 h; Irradiation;
参考文献
Su, Yijin; Zhang, Liangren; Jiao, Ning
Organic Letters, 2011 , vol. 13, # 9 p. 2168 - 2171
反应条件
potassium carbonate in acetonitrile
18 h; Ambient temperature;
参考文献
Bender, Paul E.; Hill, David T.; Offen, Priscilla H.; Razgaitis, Kazys; Lavanchy, Patricia; et al.
Journal of Medicinal Chemistry, 1985 , vol. 28, # 9 p. 1169 - 1177
反应条件
triethylamine in dichloromethane
T=20°C; 1 h;
参考文献
Koulocheri, Sophia D.; Haroutounian, Serkos A.
European Journal of Organic Chemistry, 2001 , # 9 p. 1723 - 1729
