2,6-二苯基-1,6-庚二烯合成路线 （共 8 条）
反应条件
1: AlCl3 / CH2Cl2 / 3 h / Ambient temperature 2: n-BuLi / diethyl ether; hexane / 1.) r.t., 1 h, 2.) reflux, 4 d View Scheme
参考文献
Griesbeck, Axel G.; Sadlek, Oliver; Polborn, Kurt
Liebigs Annales, 1996 , # 4 p. 545 - 549
反应条件
1: AlCl3 / CH2Cl2 / 3 h / Ambient temperature 2: n-BuLi / diethyl ether; hexane / 1.) r.t., 1 h, 2.) reflux, 4 d View Scheme
参考文献
Griesbeck, Axel G.; Sadlek, Oliver; Polborn, Kurt
Liebigs Annales, 1996 , # 4 p. 545 - 549
反应条件
ethylene glycol dimethyl ether; diethyl ether; phenyllithium Erwaermen des Reaktionsgemisches mit 1,5-Diphenyl-pentan-1,5-dion;
参考文献
Marvel; Gall
Journal of Organic Chemistry, 1959 , vol. 24, p. 1494,1495
反应条件
in 1,2-dichloro-benzene T=220.3°C; 98.4167 h; mechanism; other times and temperatures; energy data: Ea, ΔH(excit.), ΔS(excit.); Product distributionKineticsRate constant;
参考文献
Roth, Wolfgang R.; Lennartz, Hans-Werner; Doering; Birladeanu, Ludmila; Guyton, Catherine A.; Kitagawa, Toshikazu
Journal of the American Chemical Society, 1990 , vol. 112, # 5 p. 1722 - 1732
反应条件
n-butyllithium in diethyl ether; hexane 1.) r.t., 1 h, 2.) reflux, 4 d; Yield given;
参考文献
Griesbeck, Axel G.; Sadlek, Oliver; Polborn, Kurt
Liebigs Annales, 1996 , # 4 p. 545 - 549
参考文献
Posner, Gary H.; Wang, Dasong; Gonzalez, Lluisa; Tao, Xueliang; Cumming, Jared N.; Klinedinst, Donna; Shapiro, Theresa A.
Tetrahedron Letters, 1996 , vol. 37, # 6 p. 815 - 818
反应条件
1: 44 percent / 2,4,6-triphenylpyrylium tetrafluoroborate; O2 / acetonitrile / 1.08 h / Irradiation 2: 13 percent / FeBr2 / tetrahydrofuran / 4 h / 23 - 25 °C View Scheme
参考文献
Kamata, Masaki; Ohta, Motoko; Komatsu, Ken-Ichi; Kim, Hye-Sook; Wataya, Yusuke
Tetrahedron Letters, 2002 , vol. 43, # 11 p. 2063 - 2067
反应条件
anhydrous magnesium perchlorate; oxygen in acetonitrile 0.5 h; Irradiationsensitizer: DCA;
参考文献
Tetrahedron Letters, , vol. 35, # 23 p. 3953 - 3956
