1-氯-3-(2-氯乙氧基)-2-丙醇合成路线 （共 8 条）
反应条件
boron trifluoride diethyl etherate in 1,2-dichloro-ethane T=45°C; 2 h;
参考文献
Rotstein, David Mark; Melville, Chris Richard
Patent: US2008/249087 A1, 2008 ;
Location in patent: Page/Page column 35 ;
US 20080249087 A1
反应条件
boron trifluoride diethyl etherate T=45°C; Ring cleavage; 3 h;
参考文献
Romdhani, M.; Chaabouni, M. M.
Synthetic Communications, 1999 , vol. 29, # 22 p. 3939 - 3948
反应条件
tin(IV) chloride Rate constant;
参考文献
Drugov, M. V.; Barantsevich, E. N.; Smirnov P. A.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, # 6 p. 1052 - 1056
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 6 p. 1157 - 1162
参考文献
Fourneau; Ribas
Bulletin de la Societe Chimique de France, 1927 , vol. <4> 41, p. 1056
反应条件
1: 60 percent / NaOH 2: 36 percent / NaOH / H2O / 2 h / 90 °C 3: 50 percent / PCl3 View Scheme
参考文献
Tsivunin, V. S.; Zaripova, V. G.; Bikulova, V. Zh.; Zykova, V. V.; Kapustina, I. V.
Journal of Organic Chemistry USSR (English Translation), 1983 , vol. 19, # 3 p. 580
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 3 p. 660 - 661
反应条件
1: 60 percent / NaOH
2: 36 percent / NaOH / H2O / 2 h / 90 °C
View Scheme
参考文献
Tsivunin, V. S.; Zaripova, V. G.; Bikulova, V. Zh.; Zykova, V. V.; Kapustina, I. V.
Journal of Organic Chemistry USSR (English Translation), 1983 , vol. 19, # 3 p. 580
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 3 p. 660 - 661
反应条件
sodium hydroxide in water
T=20°C; Cyclization; 2 h;
参考文献
Romdhani, M.; Chaabouni, M. M.
Synthetic Communications, 1999 , vol. 29, # 22 p. 3939 - 3948
反应条件
sodium hydroxide in water
T=20 - 90°C; 5 h;
参考文献
Rotstein, David Mark; Melville, Chris Richard
Patent: US2008/249087 A1, 2008 ;
Location in patent: Page/Page column 35 ;
US 20080249087 A1
