3-(3-甲氧基苯基)-2-丙炔-1-醇合成路线 （共 4 条）
反应条件
copper(l) iodide; diisopropylamine; triphenylphosphine; palladium on activated charcoal in N,N-dimethyl-formamide T=100°C; Sonogashira reaction; 18 h;
参考文献
Soler, Roger; Cacchi, Sandro; Fabrizi, Giancarlo; Forte, Giovanni; Martin, Laura; Martinez, Sandra; Molins, Elies; Moreno-Manas, Marcial; Petrucci, Francesco; Roig, Anna; Sebastian, Rosa M.; Vallribera, Adelina
Synthesis, 2007 , # 19 p. 3068 - 3072
反应条件
1: 72 percent / diethyl azodicarboxylate, Ph3P / tetrahydrofuran / 24 h / Ambient temperature 2: 99 percent / H2NNHCH3 / CH2Cl2 / 3 h / Ambient temperature View Scheme
参考文献
Okitsu, Takashi; Sato, Kana; Potewar, Taterao M.; Wada, Akimori
Journal of Organic Chemistry, 2011 , vol. 76, # 9 p. 3438 - 3449
反应条件
manganese(IV) oxide; potassium hydroxide in benzene 0.333333 h;
参考文献
Dulog, Lothar; Koerner, Bernd; Heinze, Juergen; Yang, Jianjun
Liebigs Annalen, 1995 , # 9 p. 1663 - 1672
反应条件
5 palladium on charcoal; hydrogen in methanol
12 h; Inert atmosphere;
参考文献
Zhao, Peng; Beaudry, Christopher M.
Organic Letters, 2013 , vol. 15, # 2 p. 402 - 405
