1-(4-甲氧基苯基)-2-(甲基磺酰基)-1-乙酮合成路线 （共 7 条）
反应条件
lt;Ru(PPh3)3Cl2gt; in benzene T=120°C; 7 h;
参考文献
Kamigata, Nobumasa; Udodaira, Kumiko; Shimizu, Toshio
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 5 p. 783 - 786
反应条件
Dess-Martin periodane in acetonitrile 2.5 h; Reflux;
参考文献
Mahajan, Ulhas S.; Akamanchi, Krishnacharya G.
Synlett, 2008 , # 7 p. 987 - 990
反应条件
1: 50 percent / Et3N / dimethylformamide / 48 h / Heating 2: 55 percent / <RuCl2(PPh3)3> / benzene / 7 h / 120 °C View Scheme
参考文献
Kamigata, Nobumasa; Udodaira, Kumiko; Shimizu, Toshio
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 5 p. 783 - 786
反应条件
1: tetrahydrofuran / 0.33 h / Ambient temperature 2: 1.) CH3Li / 1.) THF, RT, 15 min, 2.) THF, RT, 3 h View Scheme
参考文献
Ibarra, C. Alvarez; Rodriguez, R. Cuervo; Monreal, M. C. Fernandez; Navarro, F. J. Garcia; Tesorero, J. Martin
Journal of Organic Chemistry, 1989 , vol. 54, # 23 p. 5620 - 5623
反应条件
sodium hydride in toluene; paraffin Heating;
参考文献
Lamm,B.; Samuelsson,B.
Acta Chemica Scandinavica (1947-1973), 1970 , vol. 24, p. 561 - 568
反应条件
methyllithium 1.) THF, RT, 15 min, 2.) THF, RT, 3 h; Yield given. Multistep reaction;
参考文献
Ibarra, C. Alvarez; Rodriguez, R. Cuervo; Monreal, M. C. Fernandez; Navarro, F. J. Garcia; Tesorero, J. Martin
Journal of Organic Chemistry, 1989 , vol. 54, # 23 p. 5620 - 5623
反应条件
p-toluenesulfinic acid lithium salt in water; N,N-dimethyl-formamide
(electrolysis);
参考文献
Lamm,B.; Samuelsson,B.
Acta Chemica Scandinavica (1947-1973), 1970 , vol. 24, p. 561 - 568
