3-氯-2-氧代丙基苯甲酸酯合成路线 （共 5 条）
反应条件
sodium hypochlorite; sodium bromide; sodium; sodium hydrogencarbonate in water; ethyl acetate
参考文献
KANEKA CORPORATION
Patent: EP1298119 A1, 2003 ;
反应条件
sodium hydrogencarbonate in N,N-dimethyl-formamide T=0 - 20°C; 15 h;
参考文献
Caselli, Emilia; Tosi, Giovanni; Forni, Arrigo; Bucciarelli, Maria; Prati, Fabio
Farmaco, 2003 , vol. 58, # 10 p. 1029 - 1032
反应条件
pyridinium chlorochromate in dichloromethane 36 h; Ambient temperature;
参考文献
Wolfe; Jin; Yang; Kim; McEachern
Canadian Journal of Chemistry, 1994 , vol. 72, # 4 p. 1051 - 1065
反应条件
1: Et3N / CH2Cl2 2: 483 mg / pyridinium chlorochromate / CH2Cl2 / 36 h / Ambient temperature View Scheme
参考文献
Wolfe; Jin; Yang; Kim; McEachern
Canadian Journal of Chemistry, 1994 , vol. 72, # 4 p. 1051 - 1065
反应条件
(i) Py, (ii) DCC, CF3CO2H, DMSO, Et2O,; Multistep reaction;
参考文献
Pero,R.W. et al.
Journal of Medicinal Chemistry, 1977 , vol. 20, p. 644 - 647
