5-苯基戊烷-2-烯-4--炔酸甲酯合成路线 （共 5 条）
反应条件
potassium carbonate; (triphenylphosphine)(2,2'-bipyridine)copper(I) bromide in toluene T=110°C; 8 h;
参考文献
Bates, Craig G.; Saejueng, Pranorm; Venkataraman
Organic Letters, 2004 , vol. 6, # 9 p. 1441 - 1444
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Saejueng, Pranorm; Bates, Craig G.; Venkataraman
Synthesis, 2005 , # 10 art. no. C03305SS, p. 1706 - 1712
反应条件
copper(l) iodide; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran; N,N-dimethyl-formamide T=20°C; Alkylation; cross-coupling;
参考文献
Dabdoub, Miguel J.; Dabdoub, Vania B.; Marino, Joseph P.
Tetrahedron Letters, 2000 , vol. 41, # 4 p. 437 - 440
反应条件
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine T=20°C;
参考文献
Bellina; Biagetti; Carpita; Rossi
Tetrahedron, 2001 , vol. 57, # 14 p. 2857 - 2870
反应条件
acetic acid; triethylamine; lithium bromide; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide multistep reaction; synthesis of other conjugated (Z)-enynes;
参考文献
Lu, Xiyan; Huang, Xiaoling; Ma, Shengming
Tetrahedron Letters, 1992 , vol. 33, # 18 p. 2535 - 2538
反应条件
1: LiOH / 20 °C
2: 30 percent / K2CO3 / Pd(PPh3)4 / acetonitrile / 22.5 h / 70 °C
View Scheme
参考文献
Rossi, Renzo; Bellina, Fabio; Biagetti, Matteo; Catanese, Antonella; Mannina, Luisa
Tetrahedron Letters, 2000 , vol. 41, # 27 p. 5281 - 5286
