反应条件
in diethyl ether addn. of (AlMe3)2 in Et2O to a soln. of dabco in Et2O, immediate pptn., refluxing (1.5 h); Schlenk techniques;; removal of solvent (vac.), removal of excess dabco by sublimation (20°C, 1E-2 torr), recrystn. (refluxing benzene, cooling to 20°C); elem. anal.;
参考文献
Bradford, Arleen M.; Bradley, Donald C.; Hursthouse, Michael B.; Motevalli, Majid
Organometallics, 1992 , vol. 11, p. 111 - 115