2,6-二苯基-3(2H-)-吡嗪酮合成路线 （共 10 条）
反应条件
pyridine; oxygen; copper diacetate; sodium carbonate in toluene
T=20 - 100°C; 12 h; chemoselective reaction;
参考文献
Liang, Lei; Yang, Guanyu; Xu, Fengrong; Niu, Yan; Sun, Qi; Xu, Ping
European Journal of Organic Chemistry, 2013 , # 27 p. 6130 - 6136
反应条件
[N,N'-bis(5-sulfonatosalicylidene)-1,2-diaminoethane]copper disodium salt; sodium carbonate in water
T=100°C; 12 h; Green chemistry;
参考文献
Liang, Lei; Wang, Wei; Xu, Fengrong; Niu, Yan; Sun, Qi; Xu, Ping
Organic Letters, 2013 , vol. 15, # 11 p. 2770 - 2773
反应条件
[N,N'-bis(5-sulfonatosalicylidene)-1,2-diaminoethane]copper disodium salt; sodium carbonate in water
T=100°C; 12 h; Green chemistry;
参考文献
Liang, Lei; Wang, Wei; Xu, Fengrong; Niu, Yan; Sun, Qi; Xu, Ping
Organic Letters, 2013 , vol. 15, # 11 p. 2770 - 2773
反应条件
[N,N'-bis(5-sulfonatosalicylidene)-1,2-diaminoethane]copper disodium salt; sodium carbonate in water
T=100°C; 12 h; Green chemistry;
参考文献
Liang, Lei; Wang, Wei; Xu, Fengrong; Niu, Yan; Sun, Qi; Xu, Ping
Organic Letters, 2013 , vol. 15, # 11 p. 2770 - 2773
反应条件
C20H10Cl2CuN2O8S2(2-)*2Na(1+); sodium carbonate in water
T=20 - 80°C; 12 h; Sealed tube;
参考文献
Liang, Lei; Wang, Wei; Wu, Jun; Xu, Fengrong; Niu, Yan; Xu, Bo; Xu, Ping
Chemistry - A European Journal, 2013 , vol. 19, # 41 p. 13774 - 13782
反应条件
2: sodium acetate
View Scheme
参考文献
Cromwell et al.
Journal of the American Chemical Society, 1956 , vol. 78, p. 4412,4415
反应条件
2: sodium acetate
View Scheme
参考文献
Cromwell et al.
Journal of the American Chemical Society, 1956 , vol. 78, p. 4412,4415
参考文献
Cromwell et al.
Journal of the American Chemical Society, 1956 , vol. 78, p. 4412,4415
反应条件
1: 89 percent / acetic acid / Heating
2: 80 percent / Br2 / acetic acid / 1 h / 80 °C
View Scheme
参考文献
Volynets, N. F.; Smartseva, I. V.; Khramova, I. V.; Pavlova, L. A.
Journal of Organic Chemistry USSR (English Translation), 1984 , p. 1604 - 1608
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 8 p. 1760 - 1764
反应条件
1: acetic acid / Reflux
2: iodine / dimethyl sulfoxide / 7 h / 100 °C
View Scheme
参考文献
Humne, Vivek T.; Konda, Shankaraiah G.; Hasanzadeh, Kamal; Lokhande, Pradeep D.
Chinese Chemical Letters, 2011 , vol. 22, # 12 p. 1435 - 1438
