(2E,4E)-5-苯基-2,4-戊二烯酸合成路线 （共 16 条）
反应条件
1: 85 percent / HCl / diethyl ether / 20 h 2: 55 percent / DIBAL-H / toluene / 3 h / 45 °C 3: 80 percent / PBr3 / diethyl ether / 1.5 h / 0 °C View Scheme
参考文献
Huang, Yange; Fananas-Mastral, Martin; Minnaard, Adriaan J.; Feringa, Ben L.
Chemical Communications, 2013 , vol. 49, # 32 p. 3309 - 3311
反应条件
anhydrous lithium acetate; silver(I) acetate; palladium diacetate; lithium chloride in N,N-dimethyl-formamide T=120°C; 6 h; Inert atmosphere;
参考文献
Yamashita, Mana; Hirano, Koji; Satoh, Tetsuya; Miura, Masahiro
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 4 p. 631 - 636
反应条件
anhydrous lithium acetate; palladium diacetate; triphenylphosphine; lithium chloride in N,N-dimethyl-formamide T=120°C; Inert atmosphere;
参考文献
Yamashita, Mana; Hirano, Koji; Satoh, Tetsuya; Miura, Masahiro
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 4 p. 631 - 636
参考文献
Koelsch; Boekelheide
Journal of the American Chemical Society, 1944 , vol. 66, p. 412,414
参考文献
Koelsch; Boekelheide
Journal of the American Chemical Society, 1944 , vol. 66, p. 412,414
反应条件
anhydrous lithium acetate; silver(I) acetate; palladium diacetate; lithium chloride in N,N-dimethyl-formamide T=120°C; 6 h; Inert atmosphere;
参考文献
Yamashita, Mana; Hirano, Koji; Satoh, Tetsuya; Miura, Masahiro
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 4 p. 631 - 636
反应条件
anhydrous lithium acetate; palladium diacetate; triphenylphosphine; lithium chloride in N,N-dimethyl-formamide T=120°C; Inert atmosphere;
参考文献
Yamashita, Mana; Hirano, Koji; Satoh, Tetsuya; Miura, Masahiro
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 4 p. 631 - 636
参考文献
Koelsch; Boekelheide
Journal of the American Chemical Society, 1944 , vol. 66, p. 412,414
参考文献
Koelsch; Boekelheide
Journal of the American Chemical Society, 1944 , vol. 66, p. 412,414
反应条件
zinc copper in methanol; water 6 h; Heating;
参考文献
Sondengam, B. Lucas; Fomum, Z. Tanee; Charles, Georges; Akam, T. Mac
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 1219 - 1222
