2-氯-1,1,3,3,3-五氟丙-1-烯合成路线 (共 46 条)
反应条件
Catalyst M-Chromium oxide T=449°C; P=773.7 Torr; variation of temperature, time, pressure; ΔHr, ΔSr; Thermodynamic dataProduct distribution;
参考文献
Coulson, D. Robert
Journal of Fluorine Chemistry, 1990 , vol. 50, # 1 p. 77 - 87
反应条件
bromine im UV-Licht;
参考文献
Misani et al.
Journal of the American Chemical Society, 1956 , vol. 78, p. 2801,2803
参考文献
Miller et al.
Industrial and Engineering Chemistry, 1947 , vol. 39, p. 402
参考文献
Henne; Whaley; Stevenson
Journal of the American Chemical Society, 1941 , vol. 63, p. 3479
反应条件
hydrogen fluoride; copper-substituted α-chromium oxide (99percent chromium/1percent copper) treated with HF
T=280°C; P=760.051 Torr; 0.00138889 h; Inert atmosphereMonel.(TM). nickel alloy tube packed with Monel.(TM). turnings;
参考文献
Rao, Velliyur Nott Mallikarjuna; Rosenfeld, H. David; Sievert, Allen; Subramoney, Shekhar
Patent: US2010/152503 A1, 2010 ;
Location in patent: Page/Page column 11 ;
反应条件
hydrogen
T=100 - 500°C; P=735.572 - 6546.59 Torr; 0.000833333 - 0.00983333 h; Combinatorial reaction / High throughput screening (HTS);
参考文献
Hedrick, Vicki E.; Boggs, Janet K.; Brandstadter, Stephan M.; Cohn, Mitchel
Patent: US2005/38302 A1, 2005 ;
Location in patent: Page/Page column 3-14 ;
反应条件
hydrogen fluoride
T=260°C; P=760.051 Torr; 0.00833333 h; Gas phase; Product distribution / selectivity;
参考文献
E.I. DUPONT DE NEMOURS AND COMPANY
Patent: WO2005/37744 A1, 2005 ;
Location in patent: Page/Page column 13-14; 15 ;
反应条件
hydrogen fluoride; chlorine; chromium cobalt oxide in nitrogen
T=300 - 400°C; P=760.051 Torr; 0.00416667 h; Gas phase; Product distribution / selectivity;
参考文献
E.I. DU PONT DE NEMOURS AND COMPANY
Patent: WO2004/18397 A1, 2004 ;
Location in patent: Page 18; 24 ;
反应条件
hydrogen fluoride; Cr(NO3)3/ZnCl2 95/5 calcined at 900 C
T=320°C; P=760.051 Torr; 0.00416667 h; Gas phase; Product distribution / selectivity;
参考文献
E.I. DUPONT DE NEMOURS AND COMPANY
Patent: WO2005/37744 A1, 2005 ;
Location in patent: Page/Page column 13-14; 15 ;
反应条件
hydrogen fluoride; catalyst from preparation example 1 (99percent Cr/1percent Cu)
T=280 - 320°C; P=760.051 Torr; 0.00138889 h; Gas phase; Product distribution / selectivity;
参考文献
E. I. DU PONT DE NEMOURS AND COMPANY
Patent: WO2007/19357 A1, 2007 ;
Location in patent: Page/Page column 12-14 ;