2-氯-1,1,3,3,3-五氟丙-1-烯合成路线 (共 46 条)
反应条件
zinc in methanol
T=50°C; 2 h; Yield given. Yields of byproduct given;
参考文献
Paleta, Oldrich; Kvicala, Jaroslav; Guenter, Jaroslav; Dedek, Vaclav
Bulletin de la Societe Chimique de France, 1986 , # 6 p. 920 - 924
反应条件
SbF3
T=200°C; unter Druck;
参考文献
Henne; Whaley; Stevenson
Journal of the American Chemical Society, 1941 , vol. 63, p. 3479
反应条件
zinc in methanol
T=50°C; 2 h; Yield given. Yields of byproduct given;
参考文献
Paleta, Oldrich; Kvicala, Jaroslav; Guenter, Jaroslav; Dedek, Vaclav
Bulletin de la Societe Chimique de France, 1986 , # 6 p. 920 - 924
反应条件
hydrogen; Ni/Cu/Cr/CaF2
T=307 - 425°C; Gas phase; Product distribution / selectivity;
参考文献
E.I. DU PONT DE NEMOURS AND COMPANY
Patent: WO2009/79525 A2, 2009 ;
Location in patent: Page/Page column 14-15 ;
参考文献
Gregory,R. et al.
Journal of the Chemical Society [Section] C: Organic, 1968 , p. 3020 - 3025
反应条件
Catalyst M-Chromium oxide
T=449°C; P=773.7 Torr; variation of temperature, time, pressure; ΔHr, ΔSr; Thermodynamic dataProduct distribution;
参考文献
Coulson, D. Robert
Journal of Fluorine Chemistry, 1990 , vol. 50, # 1 p. 77 - 87
反应条件
Catalyst M-Chromium oxide
T=449°C; P=773.7 Torr; variation of temperature, time, pressure; ΔHr, ΔSr; Thermodynamic dataProduct distribution;
参考文献
Coulson, D. Robert
Journal of Fluorine Chemistry, 1990 , vol. 50, # 1 p. 77 - 87
反应条件
Catalyst M-Chromium oxide
T=449°C; P=773.7 Torr; variation of temperature, time, pressure; ΔHr, ΔSr; Thermodynamic dataProduct distribution;
参考文献
Coulson, D. Robert
Journal of Fluorine Chemistry, 1990 , vol. 50, # 1 p. 77 - 87
参考文献
Henne; Whaley; Stevenson
Journal of the American Chemical Society, 1941 , vol. 63, p. 3479
反应条件
copper
T=500°C; P=1 Torr; MS detection; further temp.: 400 deg C; Product distribution;
参考文献
Holoch, Jan; Sundermeyer, Wolfgang
Chemische Berichte, 1986 , vol. 119, # 1 p. 269 - 278