1,1-二氯-2,3,3,3-四氟-1-丙烯合成路线 （共 28 条）
反应条件
25weight percent chromium (III) chloride on carbon treated with HF at 300-425C T=350°C; P=760.051 Torr; 0.00833333 h;
参考文献
ASAHI GLASS COMPANY, LIMITED
Patent: US2011/319676 A1, 2011 ;
Location in patent: Page/Page column 6 ;
反应条件
25weight percent chromium (III) chloride on carbon treated with HF at 300-425C T=350°C; P=760.051 Torr; 0.00833333 h;
参考文献
E. I. DU PONT DE NEMOURS AND COMPANY
Patent: WO2008/60612 A2, 2008 ;
Location in patent: Page/Page column 16-17 ;
反应条件
hydrogen fluoride; fluorinated chromium oxide T=0 - 250°C; P=750.075 Torr; Product distribution / selectivity;
参考文献
DAIKIN INDUSTRIES, LTD.; NOSE, Masatoshi; SUGIYAMA, Akinari; SUZUKI, Atsushi
Patent: WO2010/13577 A1, 2010 ;
Location in patent: Page/Page column 16-18 ;
反应条件
hydrogen fluoride; fluorinated chromium oxide T=0 - 250°C; P=750.075 Torr; Product distribution / selectivity;
参考文献
DAIKIN INDUSTRIES, LTD.; NOSE, Masatoshi; SUGIYAMA, Akinari; SUZUKI, Atsushi
Patent: WO2010/13577 A1, 2010 ;
Location in patent: Page/Page column 18-20 ;
反应条件
hydrogenchloride; hydrogen fluoride; 95percentChromium/2percentSilver Catalyst (calcined at 900 C) T=100 - 350°C; P=760.051 Torr; Product distribution / selectivity;
参考文献
E. I. DU PONT DE NEMOURS AND COMPANY
Patent: WO2008/79265 A1, 2008 ;
Location in patent: Page/Page column 12-14 ;
反应条件
potassium hydroxide; tetrabutylammomium bromide in water T=0 - 10°C; 20 h; Product distribution / selectivity;
参考文献
Asahi Glass Company, Limited
Patent: US2011/319678 A1, 2011 ;
Location in patent: Page/Page column 8 ;
反应条件
hydrogenchloride; hydrogen fluoride; 98percentChromium/2percentPalladium Catalyst (calcined at 900 C) T=100 - 400°C; P=760.051 Torr; Product distribution / selectivity;
参考文献
E. I. DU PONT DE NEMOURS AND COMPANY
Patent: WO2008/79265 A1, 2008 ;
Location in patent: Page/Page column 12-14 ;
反应条件
hydrogenchloride; hydrogen fluoride; 95percentChromium/2percentSilver Catalyst (calcined at 400 C) T=100°C; P=760.051 Torr; 6 h; Product distribution / selectivity;
参考文献
E. I. DU PONT DE NEMOURS AND COMPANY
Patent: WO2008/79265 A1, 2008 ;
Location in patent: Page/Page column 12-14 ;
反应条件
acetic acid; zinc in ethanol T=50°C; Yield given;
参考文献
Paleta, Oldrich; Kvicala, Jaroslav; Guenter, Jaroslav; Dedek, Vaclav
Bulletin de la Societe Chimique de France, 1986 , # 6 p. 920 - 924
反应条件
aluminium trichloride T=50 - 60°C;
参考文献
Park et al.
Journal of Organic Chemistry, 1958 , vol. 23, p. 1166,1168
