乙酰苯-2,3,4,5,6-d5合成路线 （共 17 条）
参考文献
Kobayashi; Hayashi; Tan; Kishi
Organic letters, 2001 , vol. 3, # 14 p. 2245 - 2248
反应条件
1: With phosphorus pentachloride T=20°C; 20 h; 2: With potassium tert-butylate in tetrahydrofuran; diethyl ether 109 h;
参考文献
Hughes; Luckhurst; Praefcke; Singer; Tearle
Molecular Crystals and Liquid Crystals, 2003 , vol. 396, p. 187 - 225
反应条件
sodium hydroxide; water-d2 in 1,4-dioxane T=20°C; 24 h;
参考文献
Kobayashi; Hayashi; Tan; Kishi
Organic letters, 2001 , vol. 3, # 14 p. 2245 - 2248
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 179 - 182
反应条件
1: 85 percent / deuterium oxide; sodium hydroxide / dioxane / 24 h / 20 °C
2: 56.7 g / sodium borodeuteride / methanol / 1 h / 0 °C
3: 70.7 g / 1 h / 20 °C
View Scheme
参考文献
Kobayashi; Hayashi; Tan; Kishi
Organic letters, 2001 , vol. 3, # 14 p. 2245 - 2248
反应条件
lithium aluminium tetrahydride
参考文献
Nakaoki, Takahiko; Kobayashi, Masamichi
Journal of Molecular Structure, 1991 , vol. 242, # 1 p. 315 - 331
反应条件
ruthenium(II)-carbonyl-tris(triphenylphosphine) dihydride in 3,3-dimethyl-butan-2-one
T=120°C; 0.0833333 h; Sealed tube;
参考文献
Hiroshima, Shun; Matsumura, Daiki; Kochi, Takuya; Kakiuchi, Fumitoshi
Organic Letters, 2010 , vol. 12, # 22 p. 5318 - 5321
