DL-3-(1-萘基)-L-丙氨酸合成路线 (共 17 条)
反应条件
1: chloroacetic acid; H2O 2: aqueous Ba(OH)2 View Scheme
参考文献
Rout
Journal of the Indian Chemical Society, 1958 , vol. 35, p. 287,289
反应条件
1: sodium amalgam; diluted KOH-solution 2: hydrochloric acid View Scheme
参考文献
Kikkoji
Biochemische Zeitschrift, 1911 , vol. 35, p. 67
反应条件
1: sodium acetate; acetic acid 2: chloroacetic acid; H2O 3: aqueous Ba(OH)2 View Scheme
参考文献
Rout
Journal of the Indian Chemical Society, 1958 , vol. 35, p. 287,289
反应条件
3.6-dioxo-2.5-bis-α-naphthylmethylene-piperazine;
参考文献
Sasaki; Kinose
Biochemische Zeitschrift, 1921 , vol. 121, p. 173
反应条件
chiral stationary phase including isopropyl-functionalized CF6 in methanol; acetic acid; triethylamine; acetonitrile T=0°C; Purification / work up;
参考文献
BOARD OF REGENTS, THE UNIVERSITY OF TEXAS SYSTEM; ARMSTRONG, Daniel, W.; PING, Sun; BREITBACH, Zachary, S.; WANG, Chunlei
Patent: WO2010/148191 A2, 2010 ;
Location in patent: Page/Page column 45-49; 61 ;
反应条件
N-ethyl-N,N-diisopropylamine in water; acetonitrile 3 h; Ambient temperature;
参考文献
Prochazka, Zdenko; Slaninova, Jirina
Collection of Czechoslovak Chemical Communications, 1995 , vol. 60, # 12 p. 2170 - 2177
反应条件
1: 89 percent / LiAlH4 / tetrahydrofuran / 12 h / Heating
2: 44 percent / dicyclohexylcarbodiimide / CH2Cl2 / 3.5 h
View Scheme
参考文献
Xie, Jian; Seto, Christopher T.
Bioorganic and Medicinal Chemistry, 2007 , vol. 15, # 1 p. 458 - 473