in diethyl ether; cyclohexane to 1-bromoadamantane (1 mmol) and TMTH (1 mmol) in Et2O at 0°C added LDA (1 mmol, in cyclohexane) under Ar, stirred for 20 min, quenched; analyzed by GLPC;
参考文献
Reimann, Werner; Kuivila, Henry G.; Farah, Dan; Apoussidis, Theodorus
Organometallics, 1987 , vol. 6, p. 557 - 565
diisobutylaluminium hydride; palladium dichloride in octane T=80 - 90°C;
参考文献
Schleyer
Journal of the American Chemical Society, 1957 , vol. 79, p. 3292
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Schleyer; Donaldson
Journal of the American Chemical Society, 1960 , vol. 82, p. 4645,4649
