magnesium; ethylene dibromide in diethyl ether T=35°C; 10 h; no mechanical stirring; Further byproducts given. Title compound not separated from byproducts;
参考文献
Molle, G.; Bauer, P.; Dubois, J. E.
Journal of Organic Chemistry, 1982 , vol. 47, # 21 p. 4120 - 4128
1: 92 percent / iodotrimethylsilane / CH2Cl2 / 24 h / Ambient temperature 2: 19 percent Chromat. / Me3SnLi / tetrahydrofuran / 0.5 h / Ambient temperature; other (trimethylstannyl)alkali reagent; also in the presence of tert-butylamine or dicyclohexylphosphine View Scheme
参考文献
Adcock, William; Clark, Christopher I.
Journal of Organic Chemistry, 1993 , vol. <26> 58, p. 7341 - 7349