反应条件
in N,N-dimethyl-formamide addn. of CrCl2*4H2O to refluxing DMF in an inert atmosphere containing ligand, refluxing for addnl. 2 min; removal from the drybox, exposing to air, evapn. to dryness, dissolution in dry CH2Cl2, column chromy., elution redbrown band (MeOH/CH2Cl2), evapn. to dryness, extn. (CH2Cl2), filtn., evapn., drying (2 d, 50°C), recrystn. (hot C6H6), elem. anal.;
参考文献
Riley, Dennis P.
Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry, 1980 , vol. 10, p. 147 - 162