3-溴-1-甲基-1H-吡咯[2,3-B]吡啶合成路线 （共 3 条）
反应条件
bromine in dichloromethane T=0 - 20°C; Bromination; 13 h;
参考文献
Tatsugi, Jiro; Zhiwei, Tong; Amano, Tomohiro; Izawa, Yasuji
Heterocycles, 2000 , vol. 53, # 5 p. 1145 - 1150
反应条件
in N,N-dimethyl-formamide T=20 - 80°C; 18 h;
参考文献
Fairley, Gary; Hall, Catherine; Greenwood, Ryan
Synlett, 2013 , vol. 24, # 5 art. no. ST-2013-D0004-L, p. 570 - 574
反应条件
1.1: sodium hydride / N,N-dimethyl-acetamide / 0.5 h 1.2: 95 percent / N,N-dimethyl-acetamide / 12 h / 20 °C 2.1: 94 percent / bromine / CH2Cl2 / 13 h / 0 - 20 °C View Scheme
参考文献
Tatsugi, Jiro; Zhiwei, Tong; Amano, Tomohiro; Izawa, Yasuji
Heterocycles, 2000 , vol. 53, # 5 p. 1145 - 1150
