1-苄基-3,5-二甲基-苯合成路线 （共 9 条）
反应条件
aluminium trichloride in chlorobenzene
Heating;
参考文献
Mathew; Bhattacharjee; Myrboh
Synthetic Communications, 1995 , vol. 25, # 12 p. 1795 - 1800
反应条件
sodium hydroxide; hydrazine hydrate; diethylene glycol
参考文献
Truce et al.
Journal of the American Chemical Society, 1958 , vol. 80, p. 3625,3629
反应条件
dichlorosilicium bis(trifluoromethanesulfonate)
T=50°C; Friedel-Crafts alkylation; 4.5 h; Title compound not separated from byproducts;
参考文献
Shiina, Isamu; Suzuki, Masahiko
Tetrahedron Letters, 2002 , vol. 43, # 36 p. 6391 - 6394
反应条件
1: sodium hydride / tetrahydrofuran / 0.5 h / 0 °C
2: boron trifluoride diethyl etherate / 2 h / 120 °C
View Scheme
参考文献
Li, Yu; Xiong, Yan; Li, Xueming; Ling, Xuege; Huang, Ruofeng; Zhang, Xiaohui; Yang, Jianchun
Green Chemistry, 2014 , vol. 16, # 6 p. 2976 - 2981
反应条件
boron trifluoride diethyl etherate
T=120°C; 2 h; Overall yield = 92 percent;
参考文献
Li, Yu; Xiong, Yan; Li, Xueming; Ling, Xuege; Huang, Ruofeng; Zhang, Xiaohui; Yang, Jianchun
Green Chemistry, 2014 , vol. 16, # 6 p. 2976 - 2981
反应条件
fired clay lt;askanitegt;
参考文献
Petrowa; Schwarz
Zhurnal Obshchei Khimii, 1950 , vol. 20, p. 2168,2169; engl. Ausg. S. 2249, 2250
反应条件
tin(IV) chloride
Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Novrocik, Jan; Novrocikova, Marta; Titz, Milos
Collection of Czechoslovak Chemical Communications, 1980 , vol. 45, # 11 p. 3140 - 3149
反应条件
Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Novrocik, Jan; Novrocikova, Marta; Titz, Milos
Collection of Czechoslovak Chemical Communications, 1980 , vol. 45, # 11 p. 3140 - 3149
反应条件
Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Novrocik, Jan; Novrocikova, Marta; Titz, Milos
Collection of Czechoslovak Chemical Communications, 1980 , vol. 45, # 11 p. 3140 - 3149
