Alpha,4-二氯苯甲醛肟合成路线 (共 54 条)
反应条件
hydrogenchloride; oxone in N,N-dimethyl-formamide 8 h; Ambient temperature;
参考文献
Bigdeli, Mohammad A.; Mahdavinia, Gholam Hossein; Jafari, Saeed
Journal of Chemical Research, 2007 , # 1 p. 26 - 28
反应条件
hydrogenchloride; sodium hypochlorite in water T=0°C; 0.333333 h;
参考文献
NISSAN CHEMICAL INDUSTRIES, LIMITED
Patent: EP1538138 A1, 2005 ;
Location in patent: Page/Page column 501 ;
反应条件
hydrogenchloride; sodium hydroxide; hydroxylamine hydrochloride; chlorine 1.) 30 min, 2.) 0 deg C; Yield given. Multistep reaction;
参考文献
Schofield, Mark H.; Sorel, Marie-Adele; Manalansan, Ryan J.; Richardson, David P.; Markgraf, J. Hodge
Magnetic Resonance in Chemistry, 2006 , vol. 44, # 9 p. 851 - 855
参考文献
Wang; Ling; Lu
Journal of Fluorine Chemistry, 2001 , vol. 111, # 2 p. 241 - 246
参考文献
Truce,W.E.; Naik,A.R.
Canadian Journal of Chemistry, 1966 , vol. 44, p. 297 - 305
反应条件
1: NaOMe / methanol / 20 °C 2: 100 percent / aq. NaOH / methanol View Scheme
参考文献
Doyle,F.P. et al.
Journal of the Chemical Society, 1963 , p. 5838 - 5845
反应条件
1: 31 percent / triethylamine / dioxane / 24 h / Ambient temperature 2: 100 percent / 1,3,5-trimethyl-benzene / 0.5 h / Heating View Scheme
参考文献
Plenkiewicz, Jan; Zdrojewski, Tadeusz
Bulletin des Societes Chimiques Belges, 1987 , vol. 96, # 9 p. 675 - 710
反应条件
1: 90 percent / aq. NaN3 / methanol 2: acetonitrile / 12 h / 20 °C View Scheme
参考文献
Rehse, Klaus; Brehme, Franziska
Archiv der Pharmazie, 2000 , vol. 333, # 6 p. 157 - 161
反应条件
Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Das, Sushanta K.; Balasubrahmanyam, S. N.
Journal of Organic Chemistry, 1983 , vol. 48, # 23 p. 4232 - 4236
反应条件
in diethyl ether 48 h; Ambient temperature;
参考文献
Tetrahedron, , vol. 53, # 5 p. 1787 - 1796