Alpha,4-二氯苯甲醛肟合成路线 （共 54 条）
反应条件
triethylamine in diethyl ether
24 h; Ambient temperature;
参考文献
Battioni,P. et al.
Bulletin de la Societe Chimique de France, 1978 , vol. <II>, p. 415 - 427
反应条件
1: 70 percent / diethyl ether / 48 h / Ambient temperature
2: triethylamine / methanol / 48 h / Ambient temperature
3: 62 percent / benzhydroximoyl chloride, 9,10-dimethylanthracene, triethylamine / methanol / 48 h / Ambient temperature; other reagents: trimethyl phosphite, p-chlorobenzhydroximoyl chloride
View Scheme
参考文献
Quadrelli, Paolo; Invernizzi, Anna Gamba; Falzoni, Mario; Caramella, Pierluigi
Tetrahedron, 1997 , vol. 53, # 5 p. 1787 - 1796
反应条件
1: 70 percent / diethyl ether / 48 h / Ambient temperature
2: 20 percent / triethylamine / methanol / 48 h / Ambient temperature
3: trimethyl phosphite / benzene / 2 h / Heating
View Scheme
参考文献
Quadrelli, Paolo; Invernizzi, Anna Gamba; Falzoni, Mario; Caramella, Pierluigi
Tetrahedron, 1997 , vol. 53, # 5 p. 1787 - 1796
反应条件
triethylamine in diethyl ether
T=0 - 20°C;
参考文献
F. HOFFMANN-LA ROCHE AG; DOTT, Pascal; HANLON, Steven Paul; HILDBRAND, Stefan; IDING, Hans; THOMAS, Andrew; WALDMEIER, Pius
Patent: WO2013/57123 A1, 2013 ;
Location in patent: Page/Page column 37 ;
反应条件
triethylamine in ethanol
T=20°C;
参考文献
FIBROGEN, INC.
Patent: WO2009/73669 A1, 2009 ;
Location in patent: Page/Page column 69 ;
WO 2009/073669 A1
反应条件
(i) Na, EtOH, (ii) /BRN= 1210991/; Multistep reaction;
参考文献
Liu, Feng; Wang, Meiyan; Teng, Xinhuan; Zhang, Peizhi; Jiang, Lin
Research on Chemical Intermediates, 2014 , vol. 40, # 4 p. 1575 - 1581
参考文献
Farley et al.
Pr. N. Dakota Acad., 1959 , vol. 13, p. 61,64
反应条件
triethylamine in diethyl ether
48 h; Ambient temperature;
参考文献
Albini, Franca Marinone; Franco, Rita De; Bandiera, Tiziano; Caramella, Pierluigi; Corsaro, Antonino; Perrini, Giancarlo
Journal of Heterocyclic Chemistry, 1989 , vol. 26, p. 757 - 761
反应条件
pyridine; E,Z-3-PhCH2-5-(4-ClC6H4CH=)-4-oxo-2-thioxo-1,3-thiazolidine
Heating;
参考文献
Kandeel, Kamal A.; Youssef, Ahmed S. A.
Molecules, 2001 , vol. 6, # 6 p. 510 - 518
反应条件
triethylamine in ethanol
参考文献
Dal Piaz,V. et al.
Synthesis, 1975 , p. 664 - 665
