2-甲基亚磺酰-1-苯乙酮合成路线 （共 25 条）
反应条件
potassium tert-butylate T=70°C; 1 h;
参考文献
Wagner, Peter J.; Lindstrom, Michael J.
Journal of the American Chemical Society, 1987 , vol. 109, # 10 p. 3062 - 3067
反应条件
1: tetrahydrofuran / 20 h / Ambient temperature 2: 1.) CH3Li / 1.) THF, RT, 40 min, 2.) THF, RT, 3 h View Scheme
参考文献
Ibarra, C. Alvarez; Rodriguez, R. Cuervo; Monreal, M. C. Fernandez; Navarro, F. J. Garcia; Tesorero, J. Martin
Journal of Organic Chemistry, 1989 , vol. 54, # 23 p. 5620 - 5623
反应条件
in dimethyl sulfoxide T=-20°C;
参考文献
Thea, Sergio; Cevasco, Giorgio
Journal of Organic Chemistry, 1988 , vol. 53, # 17 p. 4121 - 4122
反应条件
methyllithium 1.) THF, RT, 40 min, 2.) THF, RT, 3 h; Yield given. Multistep reaction;
参考文献
Ibarra, C. Alvarez; Rodriguez, R. Cuervo; Monreal, M. C. Fernandez; Navarro, F. J. Garcia; Tesorero, J. Martin
Journal of Organic Chemistry, 1989 , vol. 54, # 23 p. 5620 - 5623
参考文献
Cardellicchio, Cosimo; Omar, Omar Hassan; Naso, Francesco; Capozzi, Maria Annunziata M.; Capitelli, Francesco; Bertolasi, Valerio
Tetrahedron Asymmetry, 2006 , vol. 17, # 2 p. 223 - 229
反应条件
1: peracetic acid View Scheme
参考文献
Cardellicchio, Cosimo; Omar, Omar Hassan; Naso, Francesco; Capozzi, Maria Annunziata M.; Capitelli, Francesco; Bertolasi, Valerio
Tetrahedron Asymmetry, 2006 , vol. 17, # 2 p. 223 - 229
反应条件
in acetic acid; benzene 2 h; Heating; Yield given. Yields of byproduct given;
参考文献
Loriga, Mario; Nuvole, Antonio; Paglietti, Giuseppe
Journal of Chemical Research, Miniprint, 1989 , # 7 p. 1553 - 1566
反应条件
acetic acid in benzene 2 h; Heating;
参考文献
Journal of Heterocyclic Chemistry, , vol. 17, # 6 p. 1559 - 1561
反应条件
in ethanol Irradiation;
参考文献
Nozaki,H. et al.
Bulletin of the Chemical Society of Japan, 1972 , vol. 45, p. 856 - 859
反应条件
1: NBS / acetone / 0.08 h 2: aq. HCl / methanol / 1.) 50 deg C, 30 min; 2.) reflux, 30 min View Scheme
参考文献
Iriuchijima; Ogawa
Synthesis, 1982 , vol. No. 1, p. 41 - 42
