(1Z)-乙烯-1,2-D2合成路线 (共 38 条)
反应条件
hydrogen bromide-d1 im UV-Licht;
参考文献
Bak et al.
Acta Chemica Scandinavica (1947-1973), 1958 , vol. 12, p. 2021,2022
参考文献
Adlington, Robert M.; Baldwin, Jack E.; Rawlings, Bernard J.
Journal of the Chemical Society, Chemical Communications, 1983 , # 6 p. 290 - 292
反应条件
pumice stone; nickel
T=40 - 120°C; Hydrogenation;
参考文献
Bond
Journal of the Chemical Society, 1958 , p. 4288
反应条件
in toluene
condensing ethylene oxide to Ta-complex in toluene at -196°C, stirring at room temp. for 5 d; collecting gaseous products in -78 and -115°C cold traps, IR detn.;
参考文献
Whinnery Jr., LeRoy L.; Henling, Lawrence M.; Bereaw, John E.
Journal of the American Chemical Society, 1991 , vol. 113, # 20 p. 7575 - 7582
反应条件
1: With NaOD in water-d2
2: With palladium diacetate in water-d2
T=30°C; 18 h;
参考文献
Gordillo, Alvaro; Jesus, Ernesto de; Lopez-Mardomingo, Carmen
Journal of the American Chemical Society, 2009 , vol. 131, p. 4584 - 4585
反应条件
methanol; potassium iodide
T=59°C;
参考文献
Schubert et al.
Journal of the American Chemical Society, 1955 , vol. 77, p. 5755
反应条件
kieselguhr; nickel
T=-80°C; bei Deuterierung;
参考文献
Douglas; Rabinovitch
Journal of the American Chemical Society, 1952 , vol. 74, p. 2486,2488
反应条件
Eu(Hg); {[Mg2Mo8O22(CH3O)6(MeOH)4](2-)[Mg(MeOH)6](2+)}*6MeOH; thiophenol in methanol
T=21°C; P=120 Torr; Further byproducts given. Title compound not separated from byproducts;
参考文献
Bardina; Bazhenova; Petrova; Shilova; Shilov
Russian Chemical Bulletin, 2006 , vol. 55, # 5 p. 793 - 801
参考文献
Coyle; Ritter
Journal of the American Chemical Society, 1967 , vol. 89, p. 5739
反应条件
hydrogen oxochlorate(I), lithium salt in water
Ambient temperature;
参考文献
Vaidyanathan, Ganesan; Wilson, Joseph W.
Journal of Organic Chemistry, 1989 , vol. 54, # 8 p. 1815 - 1820