反式-2,5-二甲基哌嗪合成路线 （共 29 条）
反应条件
hydrogen; cobalt in ammonia T=200°C; P=22502.3 Torr; 3 h;
参考文献
Bayer Aktiengesellschaft
Patent: US6365741 B2, 2002 ;
Location in patent: Example 2 ;
反应条件
hydrogen; nickel T=180 - 220°C; P=11032.6 - 62518.2 Torr;
参考文献
Dow Chem.Co.
Patent: US2810722 , 1955 ;
反应条件
acetic acid; platinum Hydrogenation;
参考文献
Kipping; Pope
Journal of the Chemical Society, 1926 , p. 1077
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Stoehr
Journal fuer Praktische Chemie (Leipzig), 1893 , vol. <2> 47, p. 494,506, 508
Journal fuer Praktische Chemie (Leipzig), 1897 , vol. 55, p. 51
反应条件
rhodium contaminated with carbon T=125 - 130°C; P=25742.8 Torr; Hydrogenation;
参考文献
Dow Chem.Co.
Patent: US2843589 , 1955 ;
反应条件
1,4-dioxane; hydrogen; nickel T=200°C; P=72079.8 Torr;
参考文献
Ishiguro et al.
Yakugaku Zasshi, 1958 , vol. 78, p. 571,574
Chem.Abstr., 1958 , p. 18453
反应条件
hydrogen; nickel T=170°C; P=51485.6 Torr;
参考文献
Dow Chem.Co.
Patent: US2861994 , 1956 ;
反应条件
hydrogen; nickel T=220 - 250°C; P=48543.5 Torr;
参考文献
Sasaki
Yuki Gosei Kagaku Kyokaishi, 1958 , vol. 16, p. 614,615,617
Chem.Abstr., 1959 , p. 3234
反应条件
[{(η5-C5Me5)IrCl}2(μ-Cl)2]; sodium hydrogencarbonate in water T=140°C; 17 h; Inert atmosphereHeating; Overall yield = 90percent;
参考文献
Lorentz-Petersen, Linda L. R.; Nordstrom, Lars Ulrik; Madsen, Robert
European Journal of Organic Chemistry, 2012 , # 34 p. 6752 - 6759
反应条件
1,4-dioxane; copper oxide-chromium oxide; hydrogen P=25742.8 Torr;
参考文献
Tsuboyama et al.
Rep. Inst. phys. chem. Res. TokyoChem.Abstr., 1965 , vol. 41, p. 194,199
Rep. Inst. phys. chem. Res. TokyoChem.Abstr., 1966 , p. 14079
参考文献
Orlowa; Gawrilow
Zhurnal Obshchei Khimii, 1957 , vol. 27, p. 3314,3319; engl. Ausg. S. 3348, 3352
