4-异丙基噁唑啉-2,5-二酮合成路线 (共 12 条)
反应条件
1: chlorocarbonic acid benzyl ester; aqueous NaOH 2: PBr3 View Scheme
参考文献
Hosten, N.; Anteunis, M. J. O.
Bulletin des Societes Chimiques Belges, 1988 , vol. 97, # 1 p. 45 - 47
反应条件
in tetrahydrofuran T=40 - 50°C; 5 h;
参考文献
Daly, William H.; Poche, Drew
Tetrahedron Letters, 1988 , vol. 29, # 46 p. 5859 - 5862
反应条件
phosphorus tribromide
参考文献
Davis
Annales de Chimie (Cachan, France), 1954 , vol. <12> 9, p. 399,426
反应条件
oxygen; nitrogen(II) oxide in dimethyl sulfoxide T=50°C; 0.166667 h; Yield given;
参考文献
Collet, Helene; Bied, Catherine; Mion, Louis; Taillades, Jacques; Commeyras, Auguste
Tetrahedron Letters, 1996 , vol. 37, # 50 p. 9043 - 9046
反应条件
phosphorus tribromide
参考文献
Ben-Ishai; Katchalski
Journal of the American Chemical Society, 1952 , vol. 74, p. 3688
参考文献
Petri; Staverman
Recueil des Travaux Chimiques des Pays-Bas, 1952 , vol. 71, p. 385,393
Full Text Show Details
Hanby et al.
Journal of the Chemical Society, 1950 , p. 3009,3011
反应条件
in dichloromethane 0.166667 h; Ambient temperature; Yield given;
参考文献
Hosten, N.; Anteunis, M. J. O.
Bulletin des Societes Chimiques Belges, 1988 , vol. 97, # 1 p. 45 - 47
参考文献
Coleman
Journal of the Chemical Society, 1950 , p. 3222,3225
Full Text Show Details
Du Pont de Nemours and Co.
Patent: DE824635 , 1950 ;
DRP/DRBP Org.Chem.
反应条件
1: NMM / tetrahydrofuran / -25 - 20 °C 2: 20 percent mol DHQD-PHN; 4 Angstroem molecular sieves / diethyl ether / 22 h / 0 °C View Scheme
参考文献
Hang; Tian; Tang; Deng
Journal of the American Chemical Society, 2001 , vol. 123, # 50 p. 12696 - 12697
反应条件
1: NMM / tetrahydrofuran / -25 - 20 °C 2: 20 percent mol DHQD-PHN; 4 Angstroem molecular sieves / diethyl ether / 22 h / 0 °C View Scheme
参考文献
Hang; Tian; Tang; Deng
Journal of the American Chemical Society, 2001 , vol. 123, # 50 p. 12696 - 12697