3-十三烷基-1,2-苯二酚合成路线 (共 7 条)
反应条件
hydrogenchloride in 1,4-dioxane
10 h; Heating;
参考文献
Miyakoshi, Tetsuo; Togashi, Hiroyasu
Synthesis, 1990 , # 5 p. 407 - 410
反应条件
1: H2, aq. H2SO4 / Pd-C / ethyl acetate
2: Py*HCl / Heating
View Scheme
参考文献
Kurtz,A.P.; Dawson,C.R.
Journal of Medicinal Chemistry, 1971 , vol. 14, p. 729 - 732
反应条件
1: KOH
3: H2, aq. H2SO4 / Pd-C / ethyl acetate
4: Py*HCl / Heating
View Scheme
参考文献
Kurtz,A.P.; Dawson,C.R.
Journal of Medicinal Chemistry, 1971 , vol. 14, p. 729 - 732
反应条件
2: H2, aq. H2SO4 / Pd-C / ethyl acetate
3: Py*HCl / Heating
View Scheme
参考文献
Kurtz,A.P.; Dawson,C.R.
Journal of Medicinal Chemistry, 1971 , vol. 14, p. 729 - 732
反应条件
1: Mg / tetrahydrofuran / 3 h / Ambient temperature
2: H2, cc. sulfuric acid / 5percent Pd-C / ethyl acetate
View Scheme
参考文献
Itokawa; Totsuka; Nakahara; Maezuru; Takeya; Kondo; Inamatsu; Morita
Chemical and Pharmaceutical Bulletin, 1989 , vol. 37, # 6 p. 1619 - 1621
反应条件
1: Mg / tetrahydrofuran / 3 h / Ambient temperature
2: H2, cc. sulfuric acid / 5percent Pd-C / ethyl acetate
View Scheme
参考文献
Itokawa; Totsuka; Nakahara; Maezuru; Takeya; Kondo; Inamatsu; Morita
Chemical and Pharmaceutical Bulletin, 1989 , vol. 37, # 6 p. 1619 - 1621
反应条件
pyridine hydrochloride
Heating;
参考文献
Kurtz,A.P.; Dawson,C.R.
Journal of Medicinal Chemistry, 1971 , vol. 14, p. 729 - 732