4-叠氮基-1-氟-2-硝基苯合成路线 （共 6 条）
反应条件
sodium azide; tert.-butylnitrite in tert-butyl alcohol T=20°C; 1 h;
参考文献
Das, Jagattaran; Patil, Santoshkumar N.; Awasthi, Riti; Narasimhulu, C. Prasad; Trehan, Sanjay
Synthesis, 2005 , # 11 art. no. T15104SS, p. 1801 - 1806
反应条件
2,6-dimethylpyridine in methanol T=25°C; 15 h;
参考文献
Shangguan, Ning; Katukojvala, Sreenivas; Greenberg, Rachel; Williams, Lawrence J.
Journal of the American Chemical Society, 2003 , vol. 125, # 26 p. 7754 - 7755
反应条件
triethylamine in dimethyl sulfoxide
T=60°C; Substitution;
参考文献
Swamy, Narasimha; Addo, James K.; Ray, Rahul
Bioorganic and Medicinal Chemistry Letters, 2000 , vol. 10, # 4 p. 361 - 364
反应条件
in methanol; N,N-dimethyl-formamide
T=80°C;
参考文献
Aureli, Massimo; Prioni, Simona; Mauri, Laura; Loberto, Nicoletta; Casellato, Riccardo; Ciampa, Maria Grazia; Chigorno, Vanna; Prinetti, Alessandro; Sonnino, Sandro
Journal of Lipid Research, 2010 , vol. 51, # 4 p. 798 - 808
反应条件
in dichloromethane
24 h; Ambient temperature;
参考文献
Yoshida; Nakayama; Hatanaka; Kanaoka
Chemical and Pharmaceutical Bulletin, 1990 , vol. 38, # 4 p. 982 - 987
反应条件
sodium hydrogencarbonate; urea; sodium nitrite in hydrogenchloride; chloroform; water; ethyl acetate; Petroleum ether
参考文献
Nelson Research and Development Company
Patent: US4087609 A1, 1978 ;
