反应条件
1: triethylamine / acetonitrile / 5 h / 80 °C / |Inert atmosphere
2: pyridine / dichloromethane / 1.5 h / 20 °C / |Inert atmosphere; |Cooling with ice
3: 4,7,13,16,21,24-hexaoxa-1,10-diazabicyclo[8.8.8]hexacosane; potassium fluoride / acetonitrile / 0.08 h / 80 °C / |Sealed tube
View Scheme
参考文献
Pijarowska-Kruszyna; Jaron; Kachniarz; Kasprzak; Kowalska; Malkowski; Demphel; Dolle; Mikolajczak
Journal of Labelled Compounds and Radiopharmaceuticals, 2014 , vol. 57, # 3 p. 148 - 157
