2,2-二甲氧基-2-苯乙醇合成路线 （共 8 条）
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane T=8°C; 0.5 h;
参考文献
Huet, Francois; Pellet, Michele; Lechevallier, Andre; Conia, Jean-Marie
Journal of Chemical Research, Miniprint, 1982 , # 9 p. 2528 - 2551
反应条件
potassium carbonate in methanol 0.25 h;
参考文献
Hoffman, Robert V.; Jankowski, Bryan C.; Carr, C. Sean; Duesler, Eileen N.
Journal of Organic Chemistry, 1986 , vol. 51, # 2 p. 130 - 135
反应条件
potassium hydroxide; 2-iodosylbenzoic acid 0.5 h; Ambient temperatureovernight;
参考文献
Moriarty, Robert M.; Hou, Kwang-Chung
Tetrahedron Letters, 1984 , vol. 25, # 7 p. 691 - 694
参考文献
Tanaka,R. et al.
Tetrahedron, 1971 , vol. 27, p. 2651 - 2669
反应条件
1: toluene-4-sulfonic acid / tetrahydrofuran; water / 4.5 h / |Reflux 2: potassium carbonate; 18-crown-6 ether; oxygen / water / 10 h / 80 °C / 760.05 Torr View Scheme
参考文献
Liu, Hui; Dong, Chao; Zhang, Zeguang; Wu, Peiyu; Jiang, Xuefeng
Angewandte Chemie - International Edition, 2012 , vol. 51, # 50 p. 12570 - 12574
Angew. Chem., 2012 , vol. 124, # 50 p. 12738 - 12742,5
反应条件
sulfuric acid in chloroform
参考文献
Moriarty, Robert M.; Hou, Kwang-Chung
Tetrahedron Letters, 1984 , vol. 25, # 7 p. 691 - 694
反应条件
1: toluene-4-sulfonic acid / tetrahydrofuran; water / 4.5 h / |Reflux 2: potassium carbonate; 18-crown-6 ether; oxygen / water / 10 h / 80 °C / 760.05 Torr View Scheme
参考文献
Liu, Hui; Dong, Chao; Zhang, Zeguang; Wu, Peiyu; Jiang, Xuefeng
Angewandte Chemie - International Edition, 2012 , vol. 51, # 50 p. 12570 - 12574
Angew. Chem., 2012 , vol. 124, # 50 p. 12738 - 12742,5
反应条件
1: toluene-4-sulfonic acid / tetrahydrofuran; water / 4.5 h / |Reflux
2: potassium carbonate; 18-crown-6 ether; oxygen / water / 10 h / 80 °C / 760.05 Torr
View Scheme
参考文献
Liu, Hui; Dong, Chao; Zhang, Zeguang; Wu, Peiyu; Jiang, Xuefeng
Angewandte Chemie - International Edition, 2012 , vol. 51, # 50 p. 12570 - 12574
Angew. Chem., 2012 , vol. 124, # 50 p. 12738 - 12742,5
