2,3,4,6-四邻乙酰基-alpha-d-吡喃甘露糖氟化物合成路线 (共 18 条)
反应条件
iodine; silver fluoride in dichloromethane T=20°C; 1 h; Darkness; stereoselective reaction;
参考文献
Mugunthan; Kartha, K. P. Ravindranathan
Tetrahedron Letters, 2012 , vol. 53, # 42 p. 5631 - 5634
反应条件
Xtalfluor-E® in 1,2-dichloro-ethane 0.25 h; Inert atmosphereReflux;
参考文献
Tsegay, Sammi; Williams, Rohan J.; Williams, Spencer J.
Carbohydrate Research, 2012 , vol. 357, p. 16 - 22
反应条件
Xtalfluor-E® in 1,2-dichloro-ethane 0.5 h; Inert atmosphereReflux;
参考文献
Tsegay, Sammi; Williams, Rohan J.; Williams, Spencer J.
Carbohydrate Research, 2012 , vol. 357, p. 16 - 22
反应条件
silver tetrafluoroborate in dichloromethane T=10°C;
参考文献
Voznij, Yakov V.; Koikov, Leonid N.; Galoyan, Armen A.
Carbohydrate Research, 1984 , vol. 132, p. 339 - 341
反应条件
pyridine; hydrogen fluoride T=20°C; 4 h; Sealed vial;
参考文献
Steinmann, Andreas; Thimm, Julian; Matwiejuk, Martin; Thiem, Joachim
Macromolecules, 2010 , vol. 43, # 8 p. 3606 - 3612
反应条件
pyridine hydrogenfluoride in dichloromethane 3 h; cooling; polyethylene vessel !;
参考文献
Kraaijeveld, N. A.; Boeckel, C. A. A. van
Recueil des Travaux Chimiques des Pays-Bas, 1989 , vol. 108, # 2 p. 39 - 50
反应条件
pyridine hydrogenfluoride in acetone Ambient temperature;
参考文献
Szarek, Walter A.; Grynkiewicz, Grzegorz; Doboszewski, Bogdan; Hay, George W.
Chemistry Letters, 1984 , p. 1751 - 1754
反应条件
p-MeC6H4IF2 in dichloromethane T=-78 - 20°C; Yield given. Yields of byproduct given;
参考文献
Chambers, Richard D.; Sandford, Graham; Sparrowhawk, Matthew E.; Atherton, Malcolm J.
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 16 p. 1941 - 1944
反应条件
pyridine; hydrogen fluoride 4 h; Ambient temperature;
参考文献
Horneman, Anne Marie; Lundt, Inge
Journal of Carbohydrate Chemistry, 1995 , vol. 14, # 1 p. 1 - 8
反应条件
p-MeC6H4IF2 in dichloromethane T=-78 - 20°C; Yield given. Yields of byproduct given;
参考文献
Caddick; Gazzard; Motherwell; Wilkinson
Tetrahedron, 1996 , vol. 52, # 1 p. 149 - 156