2,3,4,6-四邻乙酰基-alpha-d-吡喃甘露糖氟化物合成路线 (共 18 条)
反应条件
1-fluoro-2-methyl-N,N-diisopropyl-propenylamine in chloroform 6 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Miethchen, Ralf; Hager, Christian; Hein, Martin
Synthesis, 1997 , # 2 p. 159 - 161
反应条件
pyridine hydrogenfluoride in toluene T=-20°C; 3 h;
参考文献
Hayashi, Masahiko; Hashimoto, Shun-ichi; Noyori, Ryoji
Chemistry Letters, 1984 , p. 1747 - 1750
参考文献
Ciba-Geigy Corporation
Patent: US5218097 A1, 1993 ;
反应条件
hydrogen fluoride T=0°C; 2 h;
参考文献
Bergamaschi, Brian A.; Hedges, John I.
Carbohydrate Research, 1996 , vol. 280, # 2 p. 345 - 350
反应条件
diethylamino-sulfur trifluoride in tetrahydrofuran Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Griffith, Marei H. E.; Hindsgaul, Ole
Carbohydrate Research, 1991 , vol. 211, # 1 p. 163 - 166
反应条件
in chloroform 6 h; Ambient temperature; Product distribution;
参考文献
Ernst, Beat.; Winkler, Tammo.
Tetrahedron Letters, 1989 , vol. 30, # 23 p. 3081 - 3084
反应条件
in chloroform 6 h; Ambient temperature; Product distribution;
参考文献
Ernst, Beat.; Winkler, Tammo.
Tetrahedron Letters, 1989 , vol. 30, # 23 p. 3081 - 3084
反应条件
1: K2CO3 / methanol / 20 °C 2: 80 percent / 4-dimethylaminopyridine / pyridine / 0 - 70 °C View Scheme
参考文献
Scott, Ian L.; Market, Robert V.; DeOrazio, Russell J.; Meckler, Harold; Kogan, Timothy P.
Carbohydrate Research, 1999 , vol. 317, # 1-4 p. 210 - 216