反应条件
1: 3,5-bis(trifluoromethyl)phenyl bromide With isopropylmagnesium chloride in tetrahydrofuran T=0°C; 3 h; Inert atmosphereGloveboxSchlenk technique; 2: DPPMCl4 in tetrahydrofuran; diethyl ether T=0 - 20°C; 12 h; Inert atmosphereGloveboxSchlenk technique;
参考文献
Hulley, Elliott B.; Welch, Kevin D.; Appel, Aaron M.; Dubois, Daniel L.; Bullock, R. Morris
Journal of the American Chemical Society, 2013 , vol. 135, # 32 p. 11736 - 11739