1,4-双(二氯化磷)丁烷合成路线 （共 4 条）
反应条件
phosphorus pentachloride in diethyl ether T=-78°C;
参考文献
Tavtorkin, Alexander N.; Toloraya, Sofia A.; Nifant'Ev, Eduard E.; Nifant'Ev, Ilya E.
Tetrahedron Letters, 2011 , vol. 52, # 7 p. 824 - 825
反应条件
phosphorus trichoride 1 h; Ambient temperature;
参考文献
Diemert, Klaus; Kuchen, Wilhelm; Kutter, Juergen
Phosphorus and Sulfur and the Related Elements, 1983 , vol. 15, p. 155 - 164
反应条件
phosphorus trichoride in diethyl ether
参考文献
Sander,M.
Chemische Berichte, 1962 , vol. 95, p. 473 - 482
反应条件
hydrogenchloride; bis(diethylamino)phosphorochloridite 1.) THF, RT, overnight, 2.) ether, RT, 2 h; Yield given. Multistep reaction;
参考文献
Langer, Falk; Puentener, Kurt; Stuermer, Rainer; Knochel, Paul
Tetrahedron Asymmetry, 1997 , vol. 8, # 5 p. 715 - 738
