2-(4-甲基亚苄基)-丙二腈合成路线 (共 33 条)
反应条件
p-tolylmethylenecyanothioacetamide; triethylamine in ethanol
Ambient temperature;
参考文献
Zohdi, Hussein F.; Rateb, Nora M.; Abdelhamid, Abdou O.
Phosphorus, Sulfur and Silicon and Related Elements, 1998 , vol. 133, p. 103 - 117
反应条件
sodium hydroxide in ethanol
Ambient temperature;
参考文献
Zohdi, Hussein F.; Rateb, Nora M.; Abdelhamid, Abdou O.
Phosphorus, Sulfur and Silicon and Related Elements, 1998 , vol. 133, p. 103 - 117
反应条件
sodium hydroxide in ethanol
Ambient temperature;
参考文献
Zohdi, Hussein F.; Rateb, Nora M.; Abdelhamid, Abdou O.
Phosphorus, Sulfur and Silicon and Related Elements, 1998 , vol. 133, p. 103 - 117
反应条件
sodium hydroxide in ethanol
Ambient temperature;
参考文献
Zohdi, Hussein F.; Rateb, Nora M.; Abdelhamid, Abdou O.
Phosphorus, Sulfur and Silicon and Related Elements, 1998 , vol. 133, p. 103 - 117
反应条件
1: methanol
2: concentrated aqueous hydrochloric acid
View Scheme
参考文献
Boehm; Grohnwald
Archiv der Pharmazie (Weinheim, Germany), 1936 , vol. 274, p. 329,341
反应条件
1: (4-methylbenzyl)malononitrile With potassium hydride in acetonitrile
T=20°C; 0.333333 h; Inert atmosphereGlovebox;
2: 4-acetylamino-2,2,6,6-tetramethylpiperidine-1-oxoammonium in acetonitrile
T=24.84°C; Inert atmosphereGlovebox; Thermodynamic data;
参考文献
Cao, Ying; Zhang, Song-Chen; Zhang, Min; Shen, Guang-Bin; Zhu, Xiao-Qing
Journal of Organic Chemistry, 2013 , vol. 78, # 14 p. 7154 - 7168
反应条件
air; silica gel
T=90°C; 0.5 h; neat (no solvent);
参考文献
Yu, Chuanming; Guo, Peng; Jin, Can; Su, Weike
Journal of Chemical Research, 2009 , # 5 p. 333 - 336
参考文献
Itoh, Kazuyoshi; Ishida, Hideaki; Chikashita, Hidenori
Chemistry Letters, 1982 , p. 1117 - 1118
反应条件
piperidine in ethanol
Heating;
参考文献
Bogdanowicz-Szwed, Krystyna; Czarny, Agnieszka
Journal fuer Praktische Chemie/Chemiker-Zeitung, 1993 , vol. 335, # 3 p. 279 - 282
反应条件
Δ1-pyrroline in ethanol
T=20°C; Substitution; 3 h;
参考文献
Ahmed; Sarmah; Longchar; Boruah; Sandhu
Synthetic Communications, 2000 , vol. 30, # 4 p. 771 - 777