1,1-二甲基丙基氯化镁合成路线 （共 67 条）
反应条件
iodine in tetrahydrofuran T=20 - 50°C; 6.33333 h;
参考文献
TAIHO PHARMACEUTICAL COMPANY LIMITED; Sasaki, Takuma; Matsuda, Akira
Patent: EP1845102 A1, 2007 ;
Location in patent: Page/Page column 21 ;
反应条件
magnesium in tetrahydrofuran T=23°C; Kinetics;
参考文献
Whitmore; Badertscher
Journal of the American Chemical Society, 1933 , vol. 55, p. 1560
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Johnson; Adkins
Journal of the American Chemical Society, 1932 , vol. 54, p. 1944
反应条件
diethyl ether Darstellung unter verschiedenen Bedingungen;
参考文献
Gilman; Zoellner
Recueil des Travaux Chimiques des Pays-Bas, 1928 , vol. 47, p. 1061
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Gilman; Zoellner; Dickey
Journal of the American Chemical Society, 1929 , vol. 51, p. 1580,1585
反应条件
1: diethyl ether 2: phosphoric acid 3: 460 - 465 °C 4: platinum/charcoal / 160 °C / Hydrogenation View Scheme
参考文献
Lewina et al.
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1951 , p. 321,325
Chem.Abstr., 1952 , p. 878
反应条件
in tetrahydrofuran; hexane
反应条件
1: diethyl ether 2: copper / 250 - 300 °C View Scheme
参考文献
Conant; Webb; Mendum
Journal of the American Chemical Society, 1929 , vol. 51, p. 1253
参考文献
Gilman; Zoellner
Recueil des Travaux Chimiques des Pays-Bas, 1928 , vol. 47, p. 1061
Full Text Show Details
Bouveault
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1904 , vol. 138, p. 1109
Bulletin de la Societe Chimique de France, 1904 , vol. <3> 31, p. 1326
反应条件
copper(l) chloride in diethyl ether
参考文献
Bauer,P.; Dubois,J.E.
Journal of the American Chemical Society, 1976 , vol. 98, # 22 p. 6999 - 7007
参考文献
Norton; Hass
Journal of the American Chemical Society, 1936 , vol. 58, p. 2148
参考文献
Pillai,C.N.; Pines,H.
Journal of the American Chemical Society, 1961 , vol. 83, p. 3274 - 3279
