1,1-二甲基丙基氯化镁合成路线 （共 67 条）
反应条件
copper(l) chloride in diethyl ether
参考文献
Katz,J.-J. et al.
Bulletin de la Societe Chimique de France, 1977 , p. 683 - 687
反应条件
1: Cu2Cl2
2: (i) Br2, (ii) PBr3, ligroin
View Scheme
参考文献
Dubois,J.-E.; Lion,C.
Comptes Rendus des Seances de l'Academie des Sciences, Serie C: Sciences Chimiques, 1975 , vol. 280, p. 217 - 219
反应条件
1: diethyl ether
2: phosphoric acid
3: 460 - 465 °C
View Scheme
参考文献
Lewina et al.
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1951 , p. 321,325
Chem.Abstr., 1952 , p. 878
参考文献
Brunner; Farmer
Journal of the Chemical Society, 1937 , p. 1045
Full Text Show Details
Nightingale; Radford; Shanholtzer
Journal of the American Chemical Society, 1942 , vol. 64, p. 1662,1665
反应条件
1: diethyl ether
2: copper / 250 - 300 °C
View Scheme
参考文献
Conant; Webb; Mendum
Journal of the American Chemical Society, 1929 , vol. 51, p. 1253
参考文献
Bouveault
Bulletin de la Societe Chimique de France, 1904 , vol. <3> 31, p. 1327
反应条件
1: CuCl / diethyl ether
2: Br2 / diethyl ether
3: (i) KOtBu, THF, tBuOH, (ii) H2O2, aq. NaOH
View Scheme
参考文献
Katz,J.-J. et al.
Bulletin de la Societe Chimique de France, 1977 , p. 683 - 687
反应条件
1: diethyl ether
2: copper / 250 - 300 °C
3: diethyl ether
View Scheme
参考文献
Conant; Webb; Mendum
Journal of the American Chemical Society, 1929 , vol. 51, p. 1253
参考文献
Whitmore et al.
Journal of the American Chemical Society, 1941 , vol. 63, p. 647
参考文献
Cram; Knight
Journal of the American Chemical Society, 1952 , vol. 74, p. 5835,5837
