1,1-二甲基丙基氯化镁合成路线 （共 67 条）
反应条件
1: (i), (ii) Br2, (iii) Mg, (iv) (oxidation)
2: CaCO3, (PhCO)2O2 / benzene / 5 h / Heating
View Scheme
参考文献
Mihailovic,M.L. et al.
Tetrahedron, 1965 , vol. 21, p. 2813 - 2821
反应条件
1: diethyl ether / -40 °C
2: nickel / 170 °C / Hydrogenation
View Scheme
参考文献
Lewina et al.
Vestnik Moskovskogo Universiteta, 1957 , vol. 12, # 3 p. 165,167,168
Chem.Abstr., 1958 , p. 6141
反应条件
1: 38 percent / CuCl / -25 °C
View Scheme
参考文献
Lachance, Pierre; Eastham, Arthur M.
Canadian Journal of Chemistry, 1981 , vol. 59, p. 2621 - 2628
反应条件
1: diethyl ether
2: hydrogen chloride / beim anschliessenden Behandeln mit wss. Salzsaeure
3: diethyl ether; mercury (II)-chloride
View Scheme
参考文献
Lewina et al.
Zhurnal Obshchei Khimii, 1959 , vol. 29, p. 2945,2948,2949;engl.Ausg.S.2906,2909,2910
反应条件
1: CuCl / diethyl ether / -35 °C
View Scheme
参考文献
Lachance, Pierre; Eastham, Arthur M.
Canadian Journal of Chemistry, 1981 , vol. 59, p. 2621 - 2628
反应条件
1: diethyl ether / anfangs unter Kuehlung, zuletzt unter Erwaermen
2: nickel / aluminium oxide / 170 °C / Hydrogenation
View Scheme
参考文献
Lewina et al.
Zhurnal Obshchei Khimii, 1958 , vol. 28, p. 2309,2311; engl.Ausg.S. 2347, 2351
Zhurnal Obshchei Khimii, 1959 , vol. 29, p. 2601,2602; engl.Ausg.S. 2565, 2567
参考文献
Whitmore; Badertscher
Journal of the American Chemical Society, 1933 , vol. 55, p. 1560
