反应条件
1: 93.4 percent / LiAlH4 / diethyl ether / 0.5 h / Heating
2: 91.6 percent / p-toluenesulfonic acid / diethyl ether / 3 h / 19 - 20 °C
3: 90.1 percent / Na / diethyl ether; xylene / 10 h / 25 - 30 °C
4: 97.8 percent / p-toluenesulfonic acid / methanol / 2 h / Heating
5: 93.8 percent / 48percent HBr / H2O; cyclohexane / 48 h / 80 °C
6: 98.6 percent / p-toluenesulfonic acid / diethyl ether / 2 h / 19 - 20 °C
7: 86.6 percent / Na / H2O; xylene; diethyl ether
8: 85.1 percent / p-toluenesulfonic acid / methanol / 2 h / Heating
View Scheme
参考文献
Rusanova, E. E.; Sebyakin, Yu. L.; Volkova, L. V.; Evstigneeva, R. P.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, p. 248 - 251
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 2 p. 279 - 282
