dilithium tetrachlorocuprate in tetrahydrofuran; diethyl ether T=-20 - 25°C; 3 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Mirviss, Stanley B.
Journal of Organic Chemistry, 1989 , vol. 54, # 8 p. 1948 - 1951
dilithium tetrachlorocuprate; ethylmagnesium bromide 1.) THF, Et2O, from -20 to -10 deg C, 2.) a) -20 deg C, 2 h, b) 25 deg C, 1 h; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Mirviss, Stanley B.
Journal of Organic Chemistry, 1989 , vol. 54, # 8 p. 1948 - 1951
dilithium tetrachlorocuprate 1.) THF, Et2O, from -20 to -10 deg C, 2.) a) -20 deg C, 2 h, b) 25 deg C, 1 h; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Mirviss, Stanley B.
Journal of Organic Chemistry, 1989 , vol. 54, # 8 p. 1948 - 1951
