反应条件
1: 82 percent / diborane / tetrahydrofuran / 1) ice bath, 1 h; 2) 12 h, reflux 2: 90 percent / DCC / CH2Cl2 / 1.5 h / -30 °C 3: NaI, NaHCO3 / acetone / 48 h / Heating 4: 53.6 percent / diborane / tetrahydrofuran / 1) 0 degC, 2 h; 2) 4 h, reflux View Scheme
参考文献
Cossec, B.; Marsura, A.; Luu-Duc, C.
Pharmazie, 1989 , vol. 44, # 9 p. 643
