1-(1-苯基乙烯基)-萘合成路线 （共 27 条）
反应条件
tert.-butylhydroperoxide; 2,9-dimethyl-1,10-phenanthroline; gold(I) chloride in water; tert-butyl alcohol T=90°C; 24 h;
参考文献
Xing, Dong; Guan, Bingtao; Cai, Guixin; Fang, Zhao; Yang, Liping; Shi, Zhangjie
Organic Letters, 2006 , vol. 8, # 4 p. 693 - 696
反应条件
potassium phosphate; PCy3∙HBF4; bis(1,5-cyclooctadiene)nickel (0) in tetrahydrofuran
T=65°C; Suzuki-Miyaura cross coupling; 18 h;
参考文献
Hansen, Anders L.; Ebran, Jean-Philippe; Gogsig, Thomas M.; Skrydstrup, Troels
Chemical Communications, 2006 , # 39 p. 4137 - 4139
反应条件
1,3-bis-(diphenylphosphino)propane; triethylamine; palladium diacetate in N,N-dimethyl-formamide
T=80°C; 24 h;
参考文献
Cabri, Walter; Candiani, Ilaria; Bedeschi, Angelo; Santi, Roberto
Journal of Organic Chemistry, 1992 , vol. 57, # 13 p. 3558 - 3563
反应条件
1,3-bis-(diphenylphosphino)propane; triethylamine; palladium diacetate in N,N-dimethyl-formamide
T=80°C; 3 h;
参考文献
Cabri, Walter; Candiani, Ilaria; Bedeschi, Angelo; Santi, Roberto
Journal of Organic Chemistry, 1992 , vol. 57, # 13 p. 3558 - 3563
反应条件
1: 1-Bromonaphthalene With magnesium in tetrahydrofuran
2: 2-bromo-2-phenyl-1-ethene With bis(acetylacetonate)nickel(II); phosphonic acid diethyl ester; zinc dibromide; 4-(N,N-dimethlyamino)pyridine in tetrahydrofuran
T=25°C; Negishi cross-coupling; 6 h;
参考文献
Gavryushin, Andrei; Kofink, Christiane; Manolikakes, Georg; Knochel, Paul
Tetrahedron, 2006 , vol. 62, # 32 p. 7521 - 7533
反应条件
bis(η3-allyl-μ-chloropalladium(II)); Tedicyp; potassium carbonate in N,N-dimethyl-formamide
T=130°C; Suzuki cross-coupling; 20 h;
参考文献
Berthiol, Florian; Doucet, Henri; Santelli, Maurice
European Journal of Organic Chemistry, 2003 , # 6 p. 1091 - 1096
反应条件
bis(η3-allyl-μ-chloropalladium(II)); tetrabutyl ammonium fluoride in tetrahydrofuran
T=60°C; 21 h;
参考文献
Hatanaka, Yasuo; Goda, Ken-ichi; Hiyama, Tamejiro
Journal of Organometallic Chemistry, 1994 , vol. 465, # 1-2 p. 97 - 100
反应条件
1,3,5,7-tetra-azatricyclo[5.1.1.13,5]decane; dnpf; bis(dibenzylideneacetone)-palladium(0) in N,N-dimethyl acetamide
T=80°C; Heck Reaction; 13 h; Inert atmosphere;
参考文献
Zou, Yinjun; Qin, Liena; Ren, Xinfeng; Lu, Yunpeng; Li, Yongxin; Zhou, Jianrong
Chemistry - A European Journal, 2013 , vol. 19, # 10 p. 3504 - 3511
反应条件
triethylamine; palladium diacetate; 2,9-dimethyl-1,10-phenanthroline in N,N-dimethyl-formamide
T=60°C; 0.8 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Cabri, Walter; Candiani, Ilaria; Bedeschi, Angelo; Santi, Roberto
Journal of Organic Chemistry, 1993 , vol. 58, # 26 p. 7421 - 7426
反应条件
potassium phosphate; Ni(PCy3)2Cl2; water in 1,4-dioxane; toluene
T=110°C; Suzuki-Miyaura coupling; 20 h; Inert atmosphere;
参考文献
Sun, Chang-Liang; Yang, Wang; Xiao, Zhou; Wu, Zhen-Hua; Li, Bi-Jie; Guan, Bing-Tao; Shi, Zhang-Jie
Chemistry - A European Journal, 2010 , vol. 16, # 20 p. 5844 - 5847
