1-氯-1,2,2,2-四氟乙烷合成路线 （共 83 条）
反应条件
hydrogen fluoride; chromium-based fluorination catalyst T=300 - 320°C; P=3000.3 Torr;
参考文献
SHOWA DENKO K.K.
Patent: WO2005/19141 A2, 2005 ;
Location in patent: Page/Page column 17 ;
反应条件
hydrogen fluoride; SbF3; SbF5 T=129 - 143°C; P=17626.8 - 19502 Torr; 4.1 h;
参考文献
RHODIA ORGANIQUE FINE LIMITED
Patent: WO2004/46071 A1, 2004 ;
Location in patent: Page column 10-11 ;
反应条件
hydrogen fluoride; SbF3; SbF5 T=125 - 139°C; P=16351.6 - 18376.8 Torr; 3.7 h;
参考文献
RHODIA ORGANIQUE FINE LIMITED
Patent: WO2004/46071 A1, 2004 ;
Location in patent: Page column 9 ;
反应条件
silicon tetrafluoride; AlCl3, aluminium chloride T=22 - 340°C; P=8517.48 - 27393.9 Torr; 8 h;
参考文献
International Isotopes Inc.
Patent: US2009/69589 A1, 2009 ;
Location in patent: Page/Page column 5-6 ;
反应条件
hydrogen fluoride Conversion of starting material;
参考文献
Nose, Masatoshi; Takahashi, Kazuhiro; Shibanuma, Takashi
Patent: US2010/268002 A1, 2010 ;
Location in patent: Page/Page column 4-5 ;
反应条件
triethylsilane; meta-chloroperoxybenzoic acid 1) 25 deg C, 1 h, 2) 80 deg C, 10 h; Yield givenYields of byproduct given;
参考文献
Honeywell International Inc.
Patent: US7026521 B1, 2006 ;
Location in patent: Page/Page column 6-7 ;
反应条件
1: With hydrogen fluoride; oxygen T=380°C; P=760.051 Torr; Inert atmosphere; 2: With hydrogenchloride T=380°C; P=760.051 Torr;
参考文献
Loustaunau; Fayolle-Romelaer; Celerier; Brunet
Journal of Fluorine Chemistry, 2011 , vol. 132, # 12 p. 1262 - 1265
反应条件
germanium tetrafluoride; AlCl3, aluminium chloride T=21 - 340°C; P=10275.8 - 41874.4 Torr; 8 h; Product distribution / selectivity;
参考文献
Omotowa, Bamidele
Patent: US2008/262276 A1, 2008 ;
Location in patent: Page/Page column 4 ;
反应条件
hydrogen fluoride; chromium oxyfluoride T=350°C; P=1125.11 Torr; Gas phase; Product distribution / selectivity;
参考文献
Nose, Masatoshi; Takahashi, Kazuhiro; Shibanuma, Takashi
Patent: US2010/268002 A1, 2010 ;
Location in patent: Page/Page column 5-6 ;
反应条件
hydrogen; palladium/alumina T=140°C; var. temp.; other catalysts; Product distributionMechanism;
参考文献
Early, Kintu; Kovalchuk, Vladimir I.; Lonyi, Ferenc; Deshmukh, Subodh; D'Itri, Julie L.
Journal of Catalysis, 1999 , vol. 182, # 1 p. 219 - 227
