(1Z)-2-偶氮基-1-乙氧基-3-氧代-3-苯基-1-丙烯-1-醇合成路线 (共 9 条)
反应条件
dirhodium(II) tetraoctanoate in dichloromethane
参考文献
Bourdon, Lisa H.; Fairfax, David J.; Martin, Gregory S.; Mathison, Casey J.; Zhichkin, Pavel
Tetrahedron Asymmetry, 2004 , vol. 15, # 22 p. 3485 - 3487
参考文献
Staudinger; Hirzel
Chemische Berichte, 1916 , vol. 49, p. 2526
反应条件
Behandeln des Reaktionsproduktes mit verd. Natriumaethylat-Loesung;
参考文献
Schroeter
Chemische Berichte, 1916 , vol. 49, p. 2704
Chemische Berichte, 1920 , vol. 53, p. 1917
反应条件
copper in benzene Oxidation;
参考文献
Hilgenkamp, Ramona; Brogan, John B.; Zercher, Charles K.
Heterocycles, 1999 , vol. 51, # 5 p. 1073 - 1078
反应条件
1: With dirhodium tetraacetate in toluene 2 h; RefluxInert atmosphere; 2: in toluene RefluxInert atmosphere;
参考文献
Honey, Mark A.; Blake, Alexander J.; Campbell, Ian B.; Judkins, Brian D.; Moody, Christopher J.
Tetrahedron, 2009 , vol. 65, # 44 p. 8995 - 9001
参考文献
Wolff; Hall
Chemische Berichte, 1903 , vol. 36, p. 3614
反应条件
HBF4*Et2O in dichloromethane
T=0 - 20°C; 5 h; Inert atmosphere; Reagent/catalystSolventTemperatureTime;
参考文献
Pasceri, Raffaele; Bartrum, Hannah E.; Hayes, Christopher J.; Moody, Christopher J.
Chemical Communications, 2012 , vol. 48, # 99 p. 12077 - 12079
反应条件
Co(C20H8N4(C6H3(C(CH3)3)2)2(C6H3(NHCOCH(CH3)2)2)2) in 1,2-dichloro-benzene
T=80°C; 24 h; Inert atmosphere; regioselective reaction;
参考文献
Cui, Xin; Xu, Xue; Wojtas, Lukasz; Kim, Martin M.; Zhang, X. Peter
Journal of the American Chemical Society, 2012 , vol. 134, # 49 p. 19981 - 19984
参考文献
Wolff; Hall
Chemische Berichte, 1903 , vol. 36, p. 3614