10,12-二十二碳二炔二酸合成路线 （共 6 条）
反应条件
oxygen; ammonium chloride; copper(l) chloride in water T=20°C;
参考文献
Eaidkong, Thichamporn; Mungkarndee, Radeemada; Phollookin, Chaiwat; Tumcharern, Gamonwarn; Sukwattanasinitt, Mongkol; Wacharasindhu, Sumrit
Journal of Materials Chemistry, 2012 , vol. 22, # 13 p. 5970 - 5977
反应条件
1: 81 percent / benzyltrimethylammonium chloride, 40percent aq. KOH / benzene / 8 h / 20 - 60 °C 2: 1.) CuCl, NH2OH*HCl, MeNH2 / 1.) methanol, 2.) methanol, 4 h View Scheme
参考文献
Radchenko, O. A.; Proshakova, E. V.; Kotlinskaya, A. N.; Il'chenko, A. Ya.
Journal of Organic Chemistry USSR (English Translation), 1991 , vol. 27, # 7.1 p. 1281 - 1290
Zhurnal Organicheskoi Khimii, 1991 , vol. 27, # 7 p. 1463 - 1473
反应条件
1: NaNH2 2: CuCl2, O2 View Scheme
参考文献
Chicoisne et al.
Bulletin de la Societe Chimique de France, 1957 , p. 1232,1236
反应条件
1: Br2 / 0 °C 2: NaNH2 3: CuCl2, O2 View Scheme
参考文献
Ozcayir, Y.; Asrar, J.; Clough, S. B.; Blumstein, A.
Molecular Crystals and Liquid Crystals (1969-1991), 1986 , vol. 138, p. 167 - 178
反应条件
hydroxylamine hydrochloride; methylamine; copper(l) chloride 1.) methanol, 2.) methanol, 4 h; Multistep reaction. Yields of byproduct given;
参考文献
Radchenko, O. A.; Proshakova, E. V.; Kotlinskaya, A. N.; Il'chenko, A. Ya.
Journal of Organic Chemistry USSR (English Translation), 1991 , vol. 27, # 7.1 p. 1281 - 1290
Zhurnal Organicheskoi Khimii, 1991 , vol. 27, # 7 p. 1463 - 1473
反应条件
Pd-BaSO4 Hydrogenation;
参考文献
Seher
Justus Liebigs Annalen der Chemie, 1954 , vol. 589, p. 222,235
Full Text Show Details
Chicoisne et al.
Bulletin de la Societe Chimique de France, 1957 , p. 1232,1236
Full Text Show Details
Black; Weedon
Journal of the Chemical Society, 1953 , p. 1785,1791
