N,N,2,4,6-戊甲基苯甲酰胺合成路线 (共 2 条)
反应条件
1: 2-Bromo-1,3,5-trimethyl-benzene With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 0.5 h; 2: N,N-dimethyl-formamide in tetrahydrofuran; hexane T=-78 - 20°C; 2 h; Further stages;
参考文献
Ushijima, Sousuke; Moriyama, Katsuhiko; Togo, Hideo
Tetrahedron, 2012 , vol. 68, # 24 p. 4701 - 4709
反应条件
bis(tri-tert-butylphosphine)palladium(0) in toluene T=100°C; 11 h;
参考文献
Cunico, Robert F.; Maity, Bikash C.
Organic Letters, 2002 , vol. 4, # 24 p. 4357 - 4359