2,2,3,3,5,5,6,6-八氟-4,4-联苯基二甲腈合成路线 （共 5 条）
反应条件
potassium phosphate; copper(l) iodide; 1,10-phenanthroline in 1,4-dioxane T=125°C; 12 h; Inert atmosphereGlovebox;
参考文献
Chen, Teng-Hao; Popov, Ilya; Zenasni, Oussama; Daugulis, Olafs; Miljanic, Ognjen S.
Chemical Communications, 2013 , vol. 49, # 61 p. 6846 - 6848
反应条件
1: With tin(ll) chloride; zinc in N,N-dimethyl-formamide Metallation; sonication; 2: With copper dichloride in N,N-dimethyl-formamide Condensation; 1 h;
参考文献
Miller, Alexey O.; Krasnov, Vyacheslav I.; Peters, Dietmar; Platonov, Vyacheslav E.; Miethchen, Ralf
Tetrahedron Letters, 2000 , vol. 41, # 20 p. 3817 - 3819
反应条件
phosphorus pentoxide T=200 - 250°C; 1.25 h;
参考文献
Efremova, N. V.; Starichenko, V. F.; Shteingarts, V. D.
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, p. 47 - 56
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 1 p. 57 - 68
反应条件
in N,N-dimethyl-formamide
参考文献
Efremova, N. V.; Starichenko, V. F.; Shteingarts, V. D.
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, p. 47 - 56
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 1 p. 57 - 68
反应条件
trifluorormethanesulfonic acid; water in trifluoroacetic acid
T=130°C; 48 h; High pressure;
参考文献
Chen, Teng-Hao; Popov, Ilya; Zenasni, Oussama; Daugulis, Olafs; Miljanic, Ognjen S.
Chemical Communications, 2013 , vol. 49, # 61 p. 6846 - 6848
