(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate; 4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl-4',4',5',5'-tetramethyl-1,3,2-dioxaborolane in dichloromethane; dimethyl sulfoxide T=85°C; 3 h; Schlenk techniqueInert atmosphere;

triethylamine; palladium on activated charcoal in carbon dioxide T=80°C; P=75006 Torr; 60 h;

triethylamine; acrylic acid methyl ester; palladium on activated charcoal in carbon dioxide T=80°C; P=75006 Torr; 60 h;

1,2-dichloro-ethane; manganese (II) chloride in tetrahydrofuran T=25°C; 12 h; Inert atmosphere;

oxygen; palladium diacetate; trifluoroacetic acid T=90 - 150°C; P=760.051 Torr; 20 h;

N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile in acetonitrile 8 h; Reflux;