反应条件
1.1: bromine / 1,4-dioxane / 0 °C 2.1: 1H-imidazole / N,N-dimethyl-formamide / 20 °C 3.1: n-butyllithium / tetrahydrofuran / -65 °C / |Inert atmosphere 3.2: 0 °C 4.1: hydrogenchloride / methanol / 20 °C / |Inert atmosphere View Scheme
参考文献
Shariatgorji, Mohammadreza; Nilsson, Anna; Goodwin, Richard J. A.; Svenningsson, Per; Schintu, Nicoletta; Banka, Zoltan; Kladni, Laszlo; Hasko, Tibor; Szabo, Andras; Andren, Per E.
Analytical Chemistry, 2012 , vol. 84, # 16 p. 7152 - 7157
