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乙二醇
甲醛
63148-62-9
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丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
补骨脂查耳酮
合成路线
（共 11 条）
1544322-43-1
→
反应条件
28448-85-3
补骨脂查耳酮
反应条件
hydrogenchloride; methanol in water T=0 - 50°C; 6 h; Inert atmosphere;
参考文献
Wang, Haomeng; Yan, Zhihong; Lei, Yanan; Sheng, Kai; Yao, Qingwei; Lu, Kui; Yu, Peng
Tetrahedron Letters, 2014 , vol. 55, # 4 p. 897 - 899
128961-13-7
→
反应条件
78316-27-5
+
28448-85-3
补骨脂查耳酮
反应条件
carbon tetrabromide in methanol 8 h; Reflux;
参考文献
Sugamoto, Kazuhiro; Matsusita, Yoh-Ichi; Matsui, Kana; Kurogi, Chiaki; Matsui, Takanao
Tetrahedron, 2011 , vol. 67, # 29 p. 5346 - 5359
89-84-9
2,4-二羟基苯乙酮
→
反应条件
28448-85-3
补骨脂查耳酮
反应条件
1: sodium hydride / dichloromethane / 2 h / 0 °C / |Inert atmosphere 2: N-iodo-succinimide / N,N-dimethyl-formamide / 10 h / 70 °C / |Inert atmosphere 3: ethanol; water / 12 h / 0 - 20 °C / |Inert atmosphere 4: caesium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / N,N-dimethyl-formamide / 2 h / 70 °C / |Inert atmosphere; |Microwave irradiation 5: hydrogenchloride; methanol / water / 6 h / 0 - 50 °C / |Inert atmosphere View Scheme
参考文献
Wang, Haomeng; Yan, Zhihong; Lei, Yanan; Sheng, Kai; Yao, Qingwei; Lu, Kui; Yu, Peng
Tetrahedron Letters, 2014 , vol. 55, # 4 p. 897 - 899
6515-05-5
→
反应条件
28448-85-3
补骨脂查耳酮
反应条件
1: N-iodo-succinimide / N,N-dimethyl-formamide / 10 h / 70 °C / |Inert atmosphere 2: ethanol; water / 12 h / 0 - 20 °C / |Inert atmosphere 3: caesium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / N,N-dimethyl-formamide / 2 h / 70 °C / |Inert atmosphere; |Microwave irradiation 4: hydrogenchloride; methanol / water / 6 h / 0 - 50 °C / |Inert atmosphere View Scheme
参考文献
Wang, Haomeng; Yan, Zhihong; Lei, Yanan; Sheng, Kai; Yao, Qingwei; Lu, Kui; Yu, Peng
Tetrahedron Letters, 2014 , vol. 55, # 4 p. 897 - 899
1544322-35-1
→
反应条件
28448-85-3
补骨脂查耳酮
反应条件
1: ethanol; water / 12 h / 0 - 20 °C / |Inert atmosphere 2: caesium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / N,N-dimethyl-formamide / 2 h / 70 °C / |Inert atmosphere; |Microwave irradiation 3: hydrogenchloride; methanol / water / 6 h / 0 - 50 °C / |Inert atmosphere View Scheme
参考文献
Wang, Haomeng; Yan, Zhihong; Lei, Yanan; Sheng, Kai; Yao, Qingwei; Lu, Kui; Yu, Peng
Tetrahedron Letters, 2014 , vol. 55, # 4 p. 897 - 899
1544322-28-2
→
反应条件
28448-85-3
补骨脂查耳酮
反应条件
1: caesium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / N,N-dimethyl-formamide / 2 h / 70 °C / |Inert atmosphere; |Microwave irradiation 2: hydrogenchloride; methanol / water / 6 h / 0 - 50 °C / |Inert atmosphere View Scheme
参考文献
Wang, Haomeng; Yan, Zhihong; Lei, Yanan; Sheng, Kai; Yao, Qingwei; Lu, Kui; Yu, Peng
Tetrahedron Letters, 2014 , vol. 55, # 4 p. 897 - 899
1092462-95-7
→
反应条件
78316-27-5
+
28448-85-3
补骨脂查耳酮
反应条件
1: montmorillonite K10 / dichloromethane / 1.5 h / 0 °C 2: hydrogenchloride / methanol; water / 3 h / Reflux View Scheme
参考文献
Sugamoto, Kazuhiro; Matsusita, Yoh-Ichi; Matsui, Kana; Kurogi, Chiaki; Matsui, Takanao
Tetrahedron, 2011 , vol. 67, # 29 p. 5346 - 5359
552-41-0
丹皮酚
→
反应条件
78316-27-5
+
28448-85-3
补骨脂查耳酮
反应条件
1: potassium carbonate / acetone / 24 h / Reflux 2: sodium hydroxide / ethanol / 12 h / 0 - 20 °C 3: montmorillonite K10 / dichloromethane / 1.5 h / 0 °C 4: hydrogenchloride / methanol; water / 3 h / Reflux View Scheme
参考文献
Sugamoto, Kazuhiro; Matsusita, Yoh-Ichi; Matsui, Kana; Kurogi, Chiaki; Matsui, Takanao
Tetrahedron, 2011 , vol. 67, # 29 p. 5346 - 5359
6515-21-5
→
反应条件
78316-27-5
+
28448-85-3
补骨脂查耳酮
反应条件
1: sodium hydroxide / ethanol / 12 h / 0 - 20 °C 2: montmorillonite K10 / dichloromethane / 1.5 h / 0 °C 3: hydrogenchloride / methanol; water / 3 h / Reflux View Scheme
参考文献
Sugamoto, Kazuhiro; Matsusita, Yoh-Ichi; Matsui, Kana; Kurogi, Chiaki; Matsui, Takanao
Tetrahedron, 2011 , vol. 67, # 29 p. 5346 - 5359
128961-25-1
→
反应条件
78316-27-5
+
28448-85-3
补骨脂查耳酮
反应条件
1: sodium hydroxide / ethanol / 12 h / 0 - 20 °C 2: montmorillonite K10 / dichloromethane / 1.5 h / 0 °C 3: hydrogenchloride / methanol; water / 3 h / Reflux View Scheme
参考文献
Sugamoto, Kazuhiro; Matsusita, Yoh-Ichi; Matsui, Kana; Kurogi, Chiaki; Matsui, Takanao
Tetrahedron, 2011 , vol. 67, # 29 p. 5346 - 5359
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